HomeMy WebLinkAboutENGINES & ENERGY CONVERSION LAB - BDR - BDR120006 - REPORTS - RECOMMENDATION/REPORT (3)Phase
II
Subsurface
Investigation
–
430
North
College
Avenue,
Fort
Collins,
Colorado
80524
December
5,
2011
National
Inspection
Services®
Commercial
&
Environmental
Stuart
Professional
Park
1136
East
Stuart
Street,
Suite
4204
Fort
Collins,
CO
80525-1193
(970)
482-1976
•
Fax
(970)
482-3388
E-mail:
bill.warren@nationalinspection.net
www.nationalinspection.net
D
ecember
5,
2011
M
r. Colorado
Stuart
State
MacMillan
University
Research
Foundation
601 Fort R
e:
South
Collins, Limited
Phase
II
Subsurface
Investigation
–
430
North
College
Avenue,
Fort
Collins,
Colorado
80524
December
5,
2011
the 2011, of
Colorado Property
arsenic,
Department
lead, by Walsh
and
Benzo(
of Environmental
Public a)pyrene
Health
were Scientists
and
identified
Environment and
in Engineers,
subsurface
Colorado LLC
soils
(CDPHE) on
in July
excess
Soil 13,
Evaluation 1.exceeded 6 mg/kg
the
Values at
standard eight
(CSEV) sampling
of
800
for
Worker
mg/locations kg
at
Standards. ranging
two
sampling from
Arsenic 4.
locations 3
exceeded mg/kg
identified –
the 20
standard mg/
at kg,
1,lead 900
Phase
II
Subsurface
Investigation
–
430
North
College
Avenue,
Fort
Collins,
Colorado
80524
December
5,
2011
ground included S
UBSURFACE surface.
in
the
CONDITIONS
enclosures A sampling
section map
of
this displaying
report. the shallow sampling locations
is
A
ccording underlying soil
profile
consists
the to
Property the
of United
fine
consist
sandy States
of
loam,
Paoli Department
sandy
fine
sandy
loam, of
loam.
and Agriculture
loamy
The
Paoli
sand. (USDA)
fine
During
sandy , the
drilling
loam soils
activities, with surface gravel
to
the
approximately and/
subsurface or clayey
Phase
II
Subsurface
Investigation
–
430
North
College
Avenue,
Fort
Collins,
Colorado
80524
December
5,
2011
National three sampling
soil
Inspection
boring points.
locations The
Services® soil
and
collected samples
a
grab
soil
one were
sample
composite
field
from
screened
soil
each
sample
of
using
the
ten
from
a
(
hand-‐10)
each
shallow
of held
the
photoionization identified results indicative below detector 10.of 0 normal part (PID) per background million meter. Results for levels. volatile The of the organic collected screening
compounds soil samples activity (VOCs)were were ,
sealed refrigeration on
November in laboratory-‐
and
10,
2011.
delivered prepared
to
Technology containers.
Laboratory, The soil
Inc. samples
Phase
II
Subsurface
Investigation
–
430
North
College
Avenue,
Fort
Collins,
Colorado
80524
December
5,
2011
CONCLUSIONS
T
his activity shallow limited
sampling identified Phase
point benzo[II subsurface
SS-‐a]8 pyrene
and
lead investigation and
above arsenic
the
CSEV above and shallow
Worker CSEV Worker subsurface
Standard Standards
in sampling
shallow
in
sampling assessment, • SS-‐the construction 8
northern point
is
National
located SS-‐
plan,
portion 10.
Inspection
at
the Based
the
northeast
of
locations
the on
Services®
Property. the
corner
of information
SS-‐
concludes 8
of
Based
and
the
SS-‐
Property
on
Phase
II
Subsurface
Investigation
–
430
North
College
Avenue,
Fort
Collins,
Colorado
80524
December
5,
2011
RELIANCE A
ll
reports,
both
verbal
and
written,
are
for
the
benefit
of
Colorado
State
University
Research by Services®. any other
Foundation. person
This or entity
report
without
has
no the
other
written
purpose consent
and
may of National
not
be
relied Inspection
upon
If report, you have
please any
contact questions
me
at regarding
your
convenience. the findings or conclusions presented in this
S
incerely, National W
illiam President bill.E
nclosures: • warren@Site
J.
Inspection
Phase
II
Subsurface
Investigation
–
430
North
College
Avenue,
Fort
Collins,
Colorado
80524
December
5,
2011
SITE
PLANS
Page 7 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
Sampled: 11/09/11
Received: 11/10/11
Laboratory ID A5091-12
Sample ID: SB-2 Project No.: Energy & Engines
Conversion Lab
Matrix: Soil
Number Parameter Result Units Method Analyzed
CAS Date
MDL
7440-39-3 Total Barium 91.6 mg/Kg 0.25 EPA-6010B 11/23/11
7440-43-9 Total Cadmium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7440-47-3 Total Chromium 11.0 mg/Kg 0.25 EPA-6010B 11/23/11
7439-92-1 Total Lead 106 mg/Kg 0.15 EPA-6010B 11/23/11
7782-49-2 Total Selenium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7740-22-4 Total Silver < 0.30 mg/Kg 0.3 EPA-6010B 11/23/11
7439-97-6 Total Mercury < 0.25 mg/Kg 0.25 EPA-7470A 11/21/11
The results contained in this report
relate only to those items tested.
Page 42 of 43
Page 52 of 80
Proposed Building Construction Area (Approx.)
NORTH
LEGEND
Soil Boring
Soil Sampling Map
Energy and Engines Conversion Lab (EECL)
430 North College Avenue
Fort Collins, Colorado 80524
National 1136 East Inspection Stuart Street, Services® Suite 4204
Fort Collins, Colorado 80525
Phone – 970-482-1976
Fax – 970-482-3388
www.nationalinspection.net
Surface Soil Sample
SS-1
SS-2
SS-3
SS-4
SS-5 SS-6
SS-7
SS-8
SS-10 SS-9
SB-1
SB-3 SB-2
Property
SOUTH
COLLEGE
AVENUE
CACHE LA POUDRE RIVER
Railroad
Right of Way
Scale: 1inch = 150 feet
EECL
BUILDING
Page 8 of 80
Proposed Building Construction Area
NORTH
LEGEND
Proposed building construction area is approximate.
Drawing not to scale
Proposed Construction Plan
Energy and Engines Conversion Lab (EECL)
430 North College Avenue
Fort Collins, Colorado 80524
National 1136 East Inspection Stuart Street, Services® Suite 4204
Fort Collins, Colorado 80525
Phone – 970-482-1976
Fax – 970-482-3388
www.nationalinspection.net
Page 9 of 80
Phase
II
Subsurface
Investigation
–
430
North
College
Avenue,
Fort
Collins,
Colorado
80524
December
5,
2011
ANALTICAL
RESULTS
Page 10 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
11/09/11
11/10/11
Laboratory ID: A5091-01
Sample ID: SS-1 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
11/15/11
Soil
µg/Kg µg/Kg µg/Kg µg/Kg
Sampled:
Received:
Analyzed:
Matrix:
110-86-1 Pyridine < 660 660 62-75-9 N-Nitrosodimethylamine < 660 660
108-95-2 Phenol < 660 660 95-57-8 2-Chlorophenol < 660 660
111-44-4 bis(-2-Chloroethyl) Ether < 660 660 541-73-1 1,3-Dichlorobenzene < 660 660
106-46-7 1,4-Dichlorobenzene < 660 660 95-50-1 1,2-Dichlorobenzene < 660 660
100-51-6 Benzyl Alcohol < 660 660 bis (2-chloroisopropyl)
Ether
108-60-1 < 660 660
95-48-7 2-Methylphenol (O-Cresol) < 660 660 621-64-7 N-Nitroso-di-n-propylamine < 660 660
67-72-1 Hexachloroethane < 660 660 3 & 4-Methylphenol (M &P-
Cresol)
< 660 660
88-75-5 2-Nitrophenol < 660 660 91-20-3 Naphthalene < 660 660
98-95-3 Nitrobenzene < 660 660 78-59-1 Isophorone < 660 660
105-67-9 2,4-Dimethylphenol < 660 660 bis(-2-
Chloroethoxy)Methane
111-91-1 < 660 660
120-83-2 2,4-Dichlorophenol < 660 660 120-82-1 1,2,4-Trichlorobenzene < 660 660
106-47-8 4-Chloroaniline < 660 660 91-57-6 2-Methylnaphthalene < 660 660
77-47-4 Hexachlorocyclopentadiene < 660 660 88-06-2 2,4,6-Trichlorophenol < 660 660
95-95-4 2,4,5-Trichlorophenol < 660 660 91-58-7 2-Chloronaphthalene < 660 660
88-74-4 2-Nitroaniline < 660 660 131-11-13 Dimethyl phthalate < 660 660
51-28-5 2,4-Dinitrophenol < 660 660 606-20-2 2,6-Dinitrotoluene < 660 660
99-09-2 3-Nitroaniline < 3300 3300 132-64-9 Dibenzofuran < 660 660
100-02-7 4-Nitrophenol < 660 660 121-14-2 2,4-Dinitrotoluene < 660 660
100-01-6 4-Nitroaniline < 3300 3300 84-66-2 Diethylphthalate < 660 660
7005-72-3 4-Chlorophenyl-phenylether < 660 660 208-96-8 Acenaphthylene < 660 660
83-32-9 Acenaphthene < 660 660 86-73-7 Fluorene < 660 660
87-86-5 Pentachlorophenol < 3300 3300 86-30-6 N-Nitrosodiphenylamine < 660 660
101-55-3 4-Bromophenyl-phenylether < 660 660 118-74-1 Hexachlorobenzene < 660 660
84-74-2 Di-n-Butylphthalate < 660 660 85-01-8 Phenanthrene < 660 660
120-12-7 Anthracene < 660 660 206-44-0 Fluoranthene < 660 660
The results contained in this report
Page 1 of 43 relate only to those items tested.
Page 11 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
Laboratory ID: A5091-01
Sample ID: SS-1 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
µg/Kg µg/Kg µg/Kg µg/Kg
85-68-7 Butylbenzylphthalate < 660 660 91-94-1 3,3'-Dichlorobenzidine < 660 660
129-00-0 Pyrene < 660 660 117-81-7 bis (2-Ethylhexyl) Phthalate < 660 660
56-55-3 Benzo[a]anthracene < 660 660 218-01-9 Chrysene < 660 660
117-84-0 Di-n-Octylphthalate < 660 660 207-flouranthene08-2 Benzo[b]< 660 660
207-08-9 Benzo[k]fluoranthene < 660 660 50-32-8 Benzo[a]pyrene < 660 660
53-70-3 Dibenzo(a,h)anthracene < 660 660 193-39-5 Indeno (1,2,3-cd) Pyrene < 660 660
191-24-2 Benzo(g,h,i)perylene < 660 660
Compound % Recovery % Rec. Limits
QA/QC SURROGATE RECOVERIES
2-Fluorophenol 93 25-121
Phenol-d5 117 24-133
Nitrobenzene-d5 69 23-120
2,4,6-Tribromophenol 94 19-122
2-Fluorobiphenyl 108 30-115
Terphenyl-d14 118 18-137
TECHNOLOGY LABORATORY, INC.
The results contained in this report
Page 2 of 43 relate only to those items tested.
Page 12 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
11/09/11
11/10/11
Laboratory ID: A5091-02
Sample ID: SS-2 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
11/15/11
Soil
µg/Kg µg/Kg µg/Kg µg/Kg
Sampled:
Received:
Analyzed:
Matrix:
110-86-1 Pyridine < 660 660 62-75-9 N-Nitrosodimethylamine < 660 660
108-95-2 Phenol < 660 660 95-57-8 2-Chlorophenol < 660 660
111-44-4 bis(-2-Chloroethyl) Ether < 660 660 541-73-1 1,3-Dichlorobenzene < 660 660
106-46-7 1,4-Dichlorobenzene < 660 660 95-50-1 1,2-Dichlorobenzene < 660 660
100-51-6 Benzyl Alcohol < 660 660 bis (2-chloroisopropyl)
Ether
108-60-1 < 660 660
95-48-7 2-Methylphenol (O-Cresol) < 660 660 621-64-7 N-Nitroso-di-n-propylamine < 660 660
67-72-1 Hexachloroethane < 660 660 3 & 4-Methylphenol (M &P-
Cresol)
< 660 660
88-75-5 2-Nitrophenol < 660 660 91-20-3 Naphthalene < 660 660
98-95-3 Nitrobenzene < 660 660 78-59-1 Isophorone < 660 660
105-67-9 2,4-Dimethylphenol < 660 660 bis(-2-
Chloroethoxy)Methane
111-91-1 < 660 660
120-83-2 2,4-Dichlorophenol < 660 660 120-82-1 1,2,4-Trichlorobenzene < 660 660
106-47-8 4-Chloroaniline < 660 660 91-57-6 2-Methylnaphthalene < 660 660
77-47-4 Hexachlorocyclopentadiene < 660 660 88-06-2 2,4,6-Trichlorophenol < 660 660
95-95-4 2,4,5-Trichlorophenol < 660 660 91-58-7 2-Chloronaphthalene < 660 660
88-74-4 2-Nitroaniline < 660 660 131-11-13 Dimethyl phthalate < 660 660
51-28-5 2,4-Dinitrophenol < 660 660 606-20-2 2,6-Dinitrotoluene < 660 660
99-09-2 3-Nitroaniline < 3300 3300 132-64-9 Dibenzofuran < 660 660
100-02-7 4-Nitrophenol < 660 660 121-14-2 2,4-Dinitrotoluene < 660 660
100-01-6 4-Nitroaniline < 3300 3300 84-66-2 Diethylphthalate < 660 660
7005-72-3 4-Chlorophenyl-phenylether < 660 660 208-96-8 Acenaphthylene < 660 660
83-32-9 Acenaphthene < 660 660 86-73-7 Fluorene < 660 660
87-86-5 Pentachlorophenol < 3300 3300 86-30-6 N-Nitrosodiphenylamine < 660 660
101-55-3 4-Bromophenyl-phenylether < 660 660 118-74-1 Hexachlorobenzene < 660 660
84-74-2 Di-n-Butylphthalate < 660 660 85-01-8 Phenanthrene < 660 660
120-12-7 Anthracene < 660 660 206-44-0 Fluoranthene < 660 660
The results contained in this report
Page 3 of 43 relate only to those items tested.
Page 13 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
Laboratory ID: A5091-02
Sample ID: SS-2 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
µg/Kg µg/Kg µg/Kg µg/Kg
85-68-7 Butylbenzylphthalate < 660 660 91-94-1 3,3'-Dichlorobenzidine < 660 660
129-00-0 Pyrene < 660 660 117-81-7 bis (2-Ethylhexyl) Phthalate < 660 660
56-55-3 Benzo[a]anthracene < 660 660 218-01-9 Chrysene < 660 660
117-84-0 Di-n-Octylphthalate < 660 660 207-flouranthene08-2 Benzo[b]< 660 660
207-08-9 Benzo[k]fluoranthene < 660 660 50-32-8 Benzo[a]pyrene < 660 660
53-70-3 Dibenzo(a,h)anthracene < 660 660 193-39-5 Indeno (1,2,3-cd) Pyrene < 660 660
191-24-2 Benzo(g,h,i)perylene < 660 660
Compound % Recovery % Rec. Limits
QA/QC SURROGATE RECOVERIES
2-Fluorophenol 85 25-121
Phenol-d5 115 24-133
Nitrobenzene-d5 94 23-120
2,4,6-Tribromophenol 47 19-122
2-Fluorobiphenyl 109 30-115
Terphenyl-d14 108 18-137
TECHNOLOGY LABORATORY, INC.
The results contained in this report
Page 4 of 43 relate only to those items tested.
Page 14 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
11/09/11
11/10/11
Laboratory ID: A5091-03
Sample ID: SS-3 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
11/15/11
Soil
µg/Kg µg/Kg µg/Kg µg/Kg
Sampled:
Received:
Analyzed:
Matrix:
110-86-1 Pyridine < 660 660 62-75-9 N-Nitrosodimethylamine < 660 660
108-95-2 Phenol < 660 660 95-57-8 2-Chlorophenol < 660 660
111-44-4 bis(-2-Chloroethyl) Ether < 660 660 541-73-1 1,3-Dichlorobenzene < 660 660
106-46-7 1,4-Dichlorobenzene < 660 660 95-50-1 1,2-Dichlorobenzene < 660 660
100-51-6 Benzyl Alcohol < 660 660 bis (2-chloroisopropyl)
Ether
108-60-1 < 660 660
95-48-7 2-Methylphenol (O-Cresol) < 660 660 621-64-7 N-Nitroso-di-n-propylamine < 660 660
67-72-1 Hexachloroethane < 660 660 3 & 4-Methylphenol (M &P-
Cresol)
< 660 660
88-75-5 2-Nitrophenol < 660 660 91-20-3 Naphthalene < 660 660
98-95-3 Nitrobenzene < 660 660 78-59-1 Isophorone < 660 660
105-67-9 2,4-Dimethylphenol < 660 660 bis(-2-
Chloroethoxy)Methane
111-91-1 < 660 660
120-83-2 2,4-Dichlorophenol < 660 660 120-82-1 1,2,4-Trichlorobenzene < 660 660
106-47-8 4-Chloroaniline < 660 660 91-57-6 2-Methylnaphthalene < 660 660
77-47-4 Hexachlorocyclopentadiene < 660 660 88-06-2 2,4,6-Trichlorophenol < 660 660
95-95-4 2,4,5-Trichlorophenol < 660 660 91-58-7 2-Chloronaphthalene < 660 660
88-74-4 2-Nitroaniline < 660 660 131-11-13 Dimethyl phthalate < 660 660
51-28-5 2,4-Dinitrophenol < 660 660 606-20-2 2,6-Dinitrotoluene < 660 660
99-09-2 3-Nitroaniline < 3300 3300 132-64-9 Dibenzofuran < 660 660
100-02-7 4-Nitrophenol < 660 660 121-14-2 2,4-Dinitrotoluene < 660 660
100-01-6 4-Nitroaniline < 3300 3300 84-66-2 Diethylphthalate < 660 660
7005-72-3 4-Chlorophenyl-phenylether < 660 660 208-96-8 Acenaphthylene < 660 660
83-32-9 Acenaphthene < 660 660 86-73-7 Fluorene < 660 660
87-86-5 Pentachlorophenol < 3300 3300 86-30-6 N-Nitrosodiphenylamine < 660 660
101-55-3 4-Bromophenyl-phenylether < 660 660 118-74-1 Hexachlorobenzene < 660 660
84-74-2 Di-n-Butylphthalate < 660 660 85-01-8 Phenanthrene < 660 660
120-12-7 Anthracene < 660 660 206-44-0 Fluoranthene < 660 660
The results contained in this report
Page 5 of 43 relate only to those items tested.
Page 15 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
Laboratory ID: A5091-03
Sample ID: SS-3 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
µg/Kg µg/Kg µg/Kg µg/Kg
85-68-7 Butylbenzylphthalate < 660 660 91-94-1 3,3'-Dichlorobenzidine < 660 660
129-00-0 Pyrene < 660 660 117-81-7 bis (2-Ethylhexyl) Phthalate < 660 660
56-55-3 Benzo[a]anthracene < 660 660 218-01-9 Chrysene < 660 660
117-84-0 Di-n-Octylphthalate < 660 660 207-flouranthene08-2 Benzo[b]< 660 660
207-08-9 Benzo[k]fluoranthene < 660 660 50-32-8 Benzo[a]pyrene < 660 660
53-70-3 Dibenzo(a,h)anthracene < 660 660 193-39-5 Indeno (1,2,3-cd) Pyrene < 660 660
191-24-2 Benzo(g,h,i)perylene < 660 660
Compound % Recovery % Rec. Limits
QA/QC SURROGATE RECOVERIES
2-Fluorophenol 95 25-121
Phenol-d5 111 24-133
Nitrobenzene-d5 87 23-120
2,4,6-Tribromophenol 48 19-122
2-Fluorobiphenyl 104 30-115
Terphenyl-d14 127 18-137
TECHNOLOGY LABORATORY, INC.
The results contained in this report
Page 6 of 43 relate only to those items tested.
Page 16 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
11/09/11
11/10/11
Laboratory ID: A5091-04
Sample ID: SS-4 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
11/15/11
Soil
µg/Kg µg/Kg µg/Kg µg/Kg
Sampled:
Received:
Analyzed:
Matrix:
110-86-1 Pyridine < 660 660 62-75-9 N-Nitrosodimethylamine < 660 660
108-95-2 Phenol < 660 660 95-57-8 2-Chlorophenol < 660 660
111-44-4 bis(-2-Chloroethyl) Ether < 660 660 541-73-1 1,3-Dichlorobenzene < 660 660
106-46-7 1,4-Dichlorobenzene < 660 660 95-50-1 1,2-Dichlorobenzene < 660 660
100-51-6 Benzyl Alcohol < 660 660 bis (2-chloroisopropyl)
Ether
108-60-1 < 660 660
95-48-7 2-Methylphenol (O-Cresol) < 660 660 621-64-7 N-Nitroso-di-n-propylamine < 660 660
67-72-1 Hexachloroethane < 660 660 3 & 4-Methylphenol (M &P-
Cresol)
< 660 660
88-75-5 2-Nitrophenol < 660 660 91-20-3 Naphthalene < 660 660
98-95-3 Nitrobenzene < 660 660 78-59-1 Isophorone < 660 660
105-67-9 2,4-Dimethylphenol < 660 660 bis(-2-
Chloroethoxy)Methane
111-91-1 < 660 660
120-83-2 2,4-Dichlorophenol < 660 660 120-82-1 1,2,4-Trichlorobenzene < 660 660
106-47-8 4-Chloroaniline < 660 660 91-57-6 2-Methylnaphthalene < 660 660
77-47-4 Hexachlorocyclopentadiene < 660 660 88-06-2 2,4,6-Trichlorophenol < 660 660
95-95-4 2,4,5-Trichlorophenol < 660 660 91-58-7 2-Chloronaphthalene < 660 660
88-74-4 2-Nitroaniline < 660 660 131-11-13 Dimethyl phthalate < 660 660
51-28-5 2,4-Dinitrophenol < 660 660 606-20-2 2,6-Dinitrotoluene < 660 660
99-09-2 3-Nitroaniline < 3300 3300 132-64-9 Dibenzofuran < 660 660
100-02-7 4-Nitrophenol < 660 660 121-14-2 2,4-Dinitrotoluene < 660 660
100-01-6 4-Nitroaniline < 3300 3300 84-66-2 Diethylphthalate < 660 660
7005-72-3 4-Chlorophenyl-phenylether < 660 660 208-96-8 Acenaphthylene < 660 660
83-32-9 Acenaphthene < 660 660 86-73-7 Fluorene < 660 660
87-86-5 Pentachlorophenol < 3300 3300 86-30-6 N-Nitrosodiphenylamine < 660 660
101-55-3 4-Bromophenyl-phenylether < 660 660 118-74-1 Hexachlorobenzene < 660 660
84-74-2 Di-n-Butylphthalate < 660 660 85-01-8 Phenanthrene < 660 660
120-12-7 Anthracene < 660 660 206-44-0 Fluoranthene < 660 660
The results contained in this report
Page 7 of 43 relate only to those items tested.
Page 17 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
Laboratory ID: A5091-04
Sample ID: SS-4 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
µg/Kg µg/Kg µg/Kg µg/Kg
85-68-7 Butylbenzylphthalate < 660 660 91-94-1 3,3'-Dichlorobenzidine < 660 660
129-00-0 Pyrene < 660 660 117-81-7 bis (2-Ethylhexyl) Phthalate < 660 660
56-55-3 Benzo[a]anthracene < 660 660 218-01-9 Chrysene < 660 660
117-84-0 Di-n-Octylphthalate < 660 660 207-flouranthene08-2 Benzo[b]< 660 660
207-08-9 Benzo[k]fluoranthene < 660 660 50-32-8 Benzo[a]pyrene < 660 660
53-70-3 Dibenzo(a,h)anthracene < 660 660 193-39-5 Indeno (1,2,3-cd) Pyrene < 660 660
191-24-2 Benzo(g,h,i)perylene < 660 660
Compound % Recovery % Rec. Limits
QA/QC SURROGATE RECOVERIES
2-Fluorophenol 86 25-121
Phenol-d5 117 24-133
Nitrobenzene-d5 63 23-120
2,4,6-Tribromophenol 45 19-122
2-Fluorobiphenyl 106 30-115
Terphenyl-d14 119 18-137
TECHNOLOGY LABORATORY, INC.
The results contained in this report
Page 8 of 43 relate only to those items tested.
Page 18 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
11/09/11
11/10/11
Laboratory ID: A5091-05
Sample ID: SS-5 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
11/15/11
Soil
µg/Kg µg/Kg µg/Kg µg/Kg
Sampled:
Received:
Analyzed:
Matrix:
110-86-1 Pyridine < 660 660 62-75-9 N-Nitrosodimethylamine < 660 660
108-95-2 Phenol < 660 660 95-57-8 2-Chlorophenol < 660 660
111-44-4 bis(-2-Chloroethyl) Ether < 660 660 541-73-1 1,3-Dichlorobenzene < 660 660
106-46-7 1,4-Dichlorobenzene < 660 660 95-50-1 1,2-Dichlorobenzene < 660 660
100-51-6 Benzyl Alcohol < 660 660 bis (2-chloroisopropyl)
Ether
108-60-1 < 660 660
95-48-7 2-Methylphenol (O-Cresol) < 660 660 621-64-7 N-Nitroso-di-n-propylamine < 660 660
67-72-1 Hexachloroethane < 660 660 3 & 4-Methylphenol (M &P-
Cresol)
< 660 660
88-75-5 2-Nitrophenol < 660 660 91-20-3 Naphthalene < 660 660
98-95-3 Nitrobenzene < 660 660 78-59-1 Isophorone < 660 660
105-67-9 2,4-Dimethylphenol < 660 660 bis(-2-
Chloroethoxy)Methane
111-91-1 < 660 660
120-83-2 2,4-Dichlorophenol < 660 660 120-82-1 1,2,4-Trichlorobenzene < 660 660
106-47-8 4-Chloroaniline < 660 660 91-57-6 2-Methylnaphthalene < 660 660
77-47-4 Hexachlorocyclopentadiene < 660 660 88-06-2 2,4,6-Trichlorophenol < 660 660
95-95-4 2,4,5-Trichlorophenol < 660 660 91-58-7 2-Chloronaphthalene < 660 660
88-74-4 2-Nitroaniline < 660 660 131-11-13 Dimethyl phthalate < 660 660
51-28-5 2,4-Dinitrophenol < 660 660 606-20-2 2,6-Dinitrotoluene < 660 660
99-09-2 3-Nitroaniline < 3300 3300 132-64-9 Dibenzofuran < 660 660
100-02-7 4-Nitrophenol < 660 660 121-14-2 2,4-Dinitrotoluene < 660 660
100-01-6 4-Nitroaniline < 3300 3300 84-66-2 Diethylphthalate < 660 660
7005-72-3 4-Chlorophenyl-phenylether < 660 660 208-96-8 Acenaphthylene < 660 660
83-32-9 Acenaphthene < 660 660 86-73-7 Fluorene < 660 660
87-86-5 Pentachlorophenol < 3300 3300 86-30-6 N-Nitrosodiphenylamine < 660 660
101-55-3 4-Bromophenyl-phenylether < 660 660 118-74-1 Hexachlorobenzene < 660 660
84-74-2 Di-n-Butylphthalate < 660 660 85-01-8 Phenanthrene < 660 660
120-12-7 Anthracene < 660 660 206-44-0 Fluoranthene < 660 660
The results contained in this report
Page 9 of 43 relate only to those items tested.
Page 19 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
Laboratory ID: A5091-05
Sample ID: SS-5 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
µg/Kg µg/Kg µg/Kg µg/Kg
85-68-7 Butylbenzylphthalate < 660 660 91-94-1 3,3'-Dichlorobenzidine < 660 660
129-00-0 Pyrene < 660 660 117-81-7 bis (2-Ethylhexyl) Phthalate < 660 660
56-55-3 Benzo[a]anthracene < 660 660 218-01-9 Chrysene < 660 660
117-84-0 Di-n-Octylphthalate < 660 660 207-flouranthene08-2 Benzo[b]< 660 660
207-08-9 Benzo[k]fluoranthene < 660 660 50-32-8 Benzo[a]pyrene < 660 660
53-70-3 Dibenzo(a,h)anthracene < 660 660 193-39-5 Indeno (1,2,3-cd) Pyrene < 660 660
191-24-2 Benzo(g,h,i)perylene < 660 660
Compound % Recovery % Rec. Limits
QA/QC SURROGATE RECOVERIES
2-Fluorophenol 96 25-121
Phenol-d5 115 24-133
Nitrobenzene-d5 71 23-120
2,4,6-Tribromophenol 58 19-122
2-Fluorobiphenyl 110 30-115
Terphenyl-d14 108 18-137
TECHNOLOGY LABORATORY, INC.
The results contained in this report
Page 10 of 43 relate only to those items tested.
Page 20 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
11/09/11
11/10/11
Laboratory ID: A5091-06
Sample ID: SS-6 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
11/16/11
Soil
µg/Kg µg/Kg µg/Kg µg/Kg
Sampled:
Received:
Analyzed:
Matrix:
110-86-1 Pyridine < 660 660 62-75-9 N-Nitrosodimethylamine < 660 660
108-95-2 Phenol < 660 660 95-57-8 2-Chlorophenol < 660 660
111-44-4 bis(-2-Chloroethyl) Ether < 660 660 541-73-1 1,3-Dichlorobenzene < 660 660
106-46-7 1,4-Dichlorobenzene < 660 660 95-50-1 1,2-Dichlorobenzene < 660 660
100-51-6 Benzyl Alcohol < 660 660 bis (2-chloroisopropyl)
Ether
108-60-1 < 660 660
95-48-7 2-Methylphenol (O-Cresol) < 660 660 621-64-7 N-Nitroso-di-n-propylamine < 660 660
67-72-1 Hexachloroethane < 660 660 3 & 4-Methylphenol (M &P-
Cresol)
< 660 660
88-75-5 2-Nitrophenol < 660 660 91-20-3 Naphthalene < 660 660
98-95-3 Nitrobenzene < 660 660 78-59-1 Isophorone < 660 660
105-67-9 2,4-Dimethylphenol < 660 660 bis(-2-
Chloroethoxy)Methane
111-91-1 < 660 660
120-83-2 2,4-Dichlorophenol < 660 660 120-82-1 1,2,4-Trichlorobenzene < 660 660
106-47-8 4-Chloroaniline < 660 660 91-57-6 2-Methylnaphthalene < 660 660
77-47-4 Hexachlorocyclopentadiene < 660 660 88-06-2 2,4,6-Trichlorophenol < 660 660
95-95-4 2,4,5-Trichlorophenol < 660 660 91-58-7 2-Chloronaphthalene < 660 660
88-74-4 2-Nitroaniline < 660 660 131-11-13 Dimethyl phthalate < 660 660
51-28-5 2,4-Dinitrophenol < 660 660 606-20-2 2,6-Dinitrotoluene < 660 660
99-09-2 3-Nitroaniline < 3300 3300 132-64-9 Dibenzofuran < 660 660
100-02-7 4-Nitrophenol < 660 660 121-14-2 2,4-Dinitrotoluene < 660 660
100-01-6 4-Nitroaniline < 3300 3300 84-66-2 Diethylphthalate < 660 660
7005-72-3 4-Chlorophenyl-phenylether < 660 660 208-96-8 Acenaphthylene < 660 660
83-32-9 Acenaphthene < 660 660 86-73-7 Fluorene < 660 660
87-86-5 Pentachlorophenol < 3300 3300 86-30-6 N-Nitrosodiphenylamine < 660 660
101-55-3 4-Bromophenyl-phenylether < 660 660 118-74-1 Hexachlorobenzene < 660 660
84-74-2 Di-n-Butylphthalate < 660 660 85-01-8 Phenanthrene 682 660
120-12-7 Anthracene < 660 660 206-44-0 Fluoranthene 1060 660
The results contained in this report
Page 11 of 43 relate only to those items tested.
Page 21 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
Laboratory ID: A5091-06
Sample ID: SS-6 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
µg/Kg µg/Kg µg/Kg µg/Kg
85-68-7 Butylbenzylphthalate < 660 660 91-94-1 3,3'-Dichlorobenzidine < 660 660
129-00-0 Pyrene 1318 660 117-81-7 bis (2-Ethylhexyl) Phthalate < 660 660
56-55-3 Benzo[a]anthracene < 660 660 218-01-9 Chrysene < 660 660
117-84-0 Di-n-Octylphthalate < 660 660 207-flouranthene08-2 Benzo[b]< 660 660
207-08-9 Benzo[k]fluoranthene < 660 660 50-32-8 Benzo[a]pyrene < 660 660
53-70-3 Dibenzo(a,h)anthracene < 660 660 193-39-5 Indeno (1,2,3-cd) Pyrene < 660 660
191-24-2 Benzo(g,h,i)perylene < 660 660
Compound % Recovery % Rec. Limits
QA/QC SURROGATE RECOVERIES
2-Fluorophenol 91 25-121
Phenol-d5 108 24-133
Nitrobenzene-d5 70 23-120
2,4,6-Tribromophenol 65 19-122
2-Fluorobiphenyl 114 30-115
Terphenyl-d14 96 18-137
TECHNOLOGY LABORATORY, INC.
The results contained in this report
Page 12 of 43 relate only to those items tested.
Page 22 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
11/09/11
11/10/11
Laboratory ID: A5091-07
Sample ID: SS-7 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
11/16/11
Soil
µg/Kg µg/Kg µg/Kg µg/Kg
Sampled:
Received:
Analyzed:
Matrix:
110-86-1 Pyridine < 660 660 62-75-9 N-Nitrosodimethylamine < 660 660
108-95-2 Phenol < 660 660 95-57-8 2-Chlorophenol < 660 660
111-44-4 bis(-2-Chloroethyl) Ether < 660 660 541-73-1 1,3-Dichlorobenzene < 660 660
106-46-7 1,4-Dichlorobenzene < 660 660 95-50-1 1,2-Dichlorobenzene < 660 660
100-51-6 Benzyl Alcohol < 660 660 bis (2-chloroisopropyl)
Ether
108-60-1 < 660 660
95-48-7 2-Methylphenol (O-Cresol) < 660 660 621-64-7 N-Nitroso-di-n-propylamine < 660 660
67-72-1 Hexachloroethane < 660 660 3 & 4-Methylphenol (M &P-
Cresol)
< 660 660
88-75-5 2-Nitrophenol < 660 660 91-20-3 Naphthalene < 660 660
98-95-3 Nitrobenzene < 660 660 78-59-1 Isophorone < 660 660
105-67-9 2,4-Dimethylphenol < 660 660 bis(-2-
Chloroethoxy)Methane
111-91-1 < 660 660
120-83-2 2,4-Dichlorophenol < 660 660 120-82-1 1,2,4-Trichlorobenzene < 660 660
106-47-8 4-Chloroaniline < 660 660 91-57-6 2-Methylnaphthalene < 660 660
77-47-4 Hexachlorocyclopentadiene < 660 660 88-06-2 2,4,6-Trichlorophenol < 660 660
95-95-4 2,4,5-Trichlorophenol < 660 660 91-58-7 2-Chloronaphthalene < 660 660
88-74-4 2-Nitroaniline < 660 660 131-11-13 Dimethyl phthalate < 660 660
51-28-5 2,4-Dinitrophenol < 660 660 606-20-2 2,6-Dinitrotoluene < 660 660
99-09-2 3-Nitroaniline < 3300 3300 132-64-9 Dibenzofuran < 660 660
100-02-7 4-Nitrophenol < 660 660 121-14-2 2,4-Dinitrotoluene < 660 660
100-01-6 4-Nitroaniline < 3300 3300 84-66-2 Diethylphthalate < 660 660
7005-72-3 4-Chlorophenyl-phenylether < 660 660 208-96-8 Acenaphthylene < 660 660
83-32-9 Acenaphthene < 660 660 86-73-7 Fluorene < 660 660
87-86-5 Pentachlorophenol < 3300 3300 86-30-6 N-Nitrosodiphenylamine < 660 660
101-55-3 4-Bromophenyl-phenylether < 660 660 118-74-1 Hexachlorobenzene < 660 660
84-74-2 Di-n-Butylphthalate < 660 660 85-01-8 Phenanthrene < 660 660
120-12-7 Anthracene < 660 660 206-44-0 Fluoranthene < 660 660
The results contained in this report
Page 13 of 43 relate only to those items tested.
Page 23 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
Laboratory ID: A5091-07
Sample ID: SS-7 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
µg/Kg µg/Kg µg/Kg µg/Kg
85-68-7 Butylbenzylphthalate < 660 660 91-94-1 3,3'-Dichlorobenzidine < 660 660
129-00-0 Pyrene < 660 660 117-81-7 bis (2-Ethylhexyl) Phthalate < 660 660
56-55-3 Benzo[a]anthracene < 660 660 218-01-9 Chrysene < 660 660
117-84-0 Di-n-Octylphthalate < 660 660 207-flouranthene08-2 Benzo[b]< 660 660
207-08-9 Benzo[k]fluoranthene < 660 660 50-32-8 Benzo[a]pyrene < 660 660
53-70-3 Dibenzo(a,h)anthracene < 660 660 193-39-5 Indeno (1,2,3-cd) Pyrene < 660 660
191-24-2 Benzo(g,h,i)perylene < 660 660
Compound % Recovery % Rec. Limits
QA/QC SURROGATE RECOVERIES
2-Fluorophenol 95 25-121
Phenol-d5 105 24-133
Nitrobenzene-d5 66 23-120
2,4,6-Tribromophenol 43 19-122
2-Fluorobiphenyl 113 30-115
Terphenyl-d14 110 18-137
TECHNOLOGY LABORATORY, INC.
The results contained in this report
Page 14 of 43 relate only to those items tested.
Page 24 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
11/09/11
11/10/11
Laboratory ID: A5091-08
Sample ID: SS-8 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
11/16/11
Soil
µg/Kg µg/Kg µg/Kg µg/Kg
Sampled:
Received:
Analyzed:
Matrix:
110-86-1 Pyridine < 660 660 62-75-9 N-Nitrosodimethylamine < 660 660
108-95-2 Phenol < 660 660 95-57-8 2-Chlorophenol < 660 660
111-44-4 bis(-2-Chloroethyl) Ether < 660 660 541-73-1 1,3-Dichlorobenzene < 660 660
106-46-7 1,4-Dichlorobenzene < 660 660 95-50-1 1,2-Dichlorobenzene < 660 660
100-51-6 Benzyl Alcohol < 660 660 bis (2-chloroisopropyl)
Ether
108-60-1 < 660 660
95-48-7 2-Methylphenol (O-Cresol) < 660 660 621-64-7 N-Nitroso-di-n-propylamine < 660 660
67-72-1 Hexachloroethane < 660 660 3 & 4-Methylphenol (M &P-
Cresol)
< 660 660
88-75-5 2-Nitrophenol < 660 660 91-20-3 Naphthalene < 660 660
98-95-3 Nitrobenzene < 660 660 78-59-1 Isophorone < 660 660
105-67-9 2,4-Dimethylphenol < 660 660 bis(-2-
Chloroethoxy)Methane
111-91-1 < 660 660
120-83-2 2,4-Dichlorophenol < 660 660 120-82-1 1,2,4-Trichlorobenzene < 660 660
106-47-8 4-Chloroaniline < 660 660 91-57-6 2-Methylnaphthalene < 660 660
77-47-4 Hexachlorocyclopentadiene < 660 660 88-06-2 2,4,6-Trichlorophenol < 660 660
95-95-4 2,4,5-Trichlorophenol < 660 660 91-58-7 2-Chloronaphthalene < 660 660
88-74-4 2-Nitroaniline < 660 660 131-11-13 Dimethyl phthalate < 660 660
51-28-5 2,4-Dinitrophenol < 660 660 606-20-2 2,6-Dinitrotoluene < 660 660
99-09-2 3-Nitroaniline < 3300 3300 132-64-9 Dibenzofuran < 660 660
100-02-7 4-Nitrophenol < 660 660 121-14-2 2,4-Dinitrotoluene < 660 660
100-01-6 4-Nitroaniline < 3300 3300 84-66-2 Diethylphthalate < 660 660
7005-72-3 4-Chlorophenyl-phenylether < 660 660 208-96-8 Acenaphthylene < 660 660
83-32-9 Acenaphthene < 660 660 86-73-7 Fluorene < 660 660
87-86-5 Pentachlorophenol < 3300 3300 86-30-6 N-Nitrosodiphenylamine < 660 660
101-55-3 4-Bromophenyl-phenylether < 660 660 118-74-1 Hexachlorobenzene < 660 660
84-74-2 Di-n-Butylphthalate < 660 660 85-01-8 Phenanthrene 1760 660
120-12-7 Anthracene < 660 660 206-44-0 Fluoranthene 3931 660
The results contained in this report
Page 15 of 43 relate only to those items tested.
Page 25 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
Laboratory ID: A5091-08
Sample ID: SS-8 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
µg/Kg µg/Kg µg/Kg µg/Kg
85-68-7 Butylbenzylphthalate < 660 660 91-94-1 3,3'-Dichlorobenzidine < 660 660
129-00-0 Pyrene 3005 660 117-81-7 bis (2-Ethylhexyl) Phthalate < 660 660
56-55-3 Benzo[a]anthracene 1066 660 218-01-9 Chrysene 1258 660
117-84-0 Di-n-Octylphthalate < 660 660 207-flouranthene08-2 Benzo[b]1625 660
207-08-9 Benzo[k]fluoranthene < 660 660 50-32-8 Benzo[a]pyrene 847 660
53-70-3 Dibenzo(a,h)anthracene < 660 660 193-39-5 Indeno (1,2,3-cd) Pyrene < 660 660
191-24-2 Benzo(g,h,i)perylene < 660 660
Compound % Recovery % Rec. Limits
QA/QC SURROGATE RECOVERIES
2-Fluorophenol 93 25-121
Phenol-d5 125 24-133
Nitrobenzene-d5 69 23-120
2,4,6-Tribromophenol 51 19-122
2-Fluorobiphenyl 111 30-115
Terphenyl-d14 106 18-137
TECHNOLOGY LABORATORY, INC.
The results contained in this report
Page 16 of 43 relate only to those items tested.
Page 26 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
11/09/11
11/10/11
Laboratory ID: A5091-09
Sample ID: SS-9 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
11/16/11
Soil
µg/Kg µg/Kg µg/Kg µg/Kg
Sampled:
Received:
Analyzed:
Matrix:
110-86-1 Pyridine < 660 660 62-75-9 N-Nitrosodimethylamine < 660 660
108-95-2 Phenol < 660 660 95-57-8 2-Chlorophenol < 660 660
111-44-4 bis(-2-Chloroethyl) Ether < 660 660 541-73-1 1,3-Dichlorobenzene < 660 660
106-46-7 1,4-Dichlorobenzene < 660 660 95-50-1 1,2-Dichlorobenzene < 660 660
100-51-6 Benzyl Alcohol < 660 660 bis (2-chloroisopropyl)
Ether
108-60-1 < 660 660
95-48-7 2-Methylphenol (O-Cresol) < 660 660 621-64-7 N-Nitroso-di-n-propylamine < 660 660
67-72-1 Hexachloroethane < 660 660 3 & 4-Methylphenol (M &P-
Cresol)
< 660 660
88-75-5 2-Nitrophenol < 660 660 91-20-3 Naphthalene < 660 660
98-95-3 Nitrobenzene < 660 660 78-59-1 Isophorone < 660 660
105-67-9 2,4-Dimethylphenol < 660 660 bis(-2-
Chloroethoxy)Methane
111-91-1 < 660 660
120-83-2 2,4-Dichlorophenol < 660 660 120-82-1 1,2,4-Trichlorobenzene < 660 660
106-47-8 4-Chloroaniline < 660 660 91-57-6 2-Methylnaphthalene < 660 660
77-47-4 Hexachlorocyclopentadiene < 660 660 88-06-2 2,4,6-Trichlorophenol < 660 660
95-95-4 2,4,5-Trichlorophenol < 660 660 91-58-7 2-Chloronaphthalene < 660 660
88-74-4 2-Nitroaniline < 660 660 131-11-13 Dimethyl phthalate < 660 660
51-28-5 2,4-Dinitrophenol < 660 660 606-20-2 2,6-Dinitrotoluene < 660 660
99-09-2 3-Nitroaniline < 3300 3300 132-64-9 Dibenzofuran < 660 660
100-02-7 4-Nitrophenol < 660 660 121-14-2 2,4-Dinitrotoluene < 660 660
100-01-6 4-Nitroaniline < 3300 3300 84-66-2 Diethylphthalate < 660 660
7005-72-3 4-Chlorophenyl-phenylether < 660 660 208-96-8 Acenaphthylene < 660 660
83-32-9 Acenaphthene < 660 660 86-73-7 Fluorene < 660 660
87-86-5 Pentachlorophenol < 3300 3300 86-30-6 N-Nitrosodiphenylamine < 660 660
101-55-3 4-Bromophenyl-phenylether < 660 660 118-74-1 Hexachlorobenzene < 660 660
84-74-2 Di-n-Butylphthalate < 660 660 85-01-8 Phenanthrene 778 660
120-12-7 Anthracene < 660 660 206-44-0 Fluoranthene 1083 660
The results contained in this report
Page 17 of 43 relate only to those items tested.
Page 27 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
Laboratory ID: A5091-09
Sample ID: SS-9 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
µg/Kg µg/Kg µg/Kg µg/Kg
85-68-7 Butylbenzylphthalate < 660 660 91-94-1 3,3'-Dichlorobenzidine < 660 660
129-00-0 Pyrene 1138 660 117-81-7 bis (2-Ethylhexyl) Phthalate < 660 660
56-55-3 Benzo[a]anthracene < 660 660 218-01-9 Chrysene < 660 660
117-84-0 Di-n-Octylphthalate < 660 660 207-flouranthene08-2 Benzo[b]< 660 660
207-08-9 Benzo[k]fluoranthene < 660 660 50-32-8 Benzo[a]pyrene < 660 660
53-70-3 Dibenzo(a,h)anthracene < 660 660 193-39-5 Indeno (1,2,3-cd) Pyrene < 660 660
191-24-2 Benzo(g,h,i)perylene < 660 660
Compound % Recovery % Rec. Limits
QA/QC SURROGATE RECOVERIES
2-Fluorophenol 92 25-121
Phenol-d5 113 24-133
Nitrobenzene-d5 73 23-120
2,4,6-Tribromophenol 67 19-122
2-Fluorobiphenyl 111 30-115
Terphenyl-d14 108 18-137
TECHNOLOGY LABORATORY, INC.
The results contained in this report
Page 18 of 43 relate only to those items tested.
Page 28 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
11/09/11
11/10/11
Laboratory ID: A5091-10
Sample ID: SS-10 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
11/16/11
Soil
µg/Kg µg/Kg µg/Kg µg/Kg
Sampled:
Received:
Analyzed:
Matrix:
110-86-1 Pyridine < 660 660 62-75-9 N-Nitrosodimethylamine < 660 660
108-95-2 Phenol < 660 660 95-57-8 2-Chlorophenol < 660 660
111-44-4 bis(-2-Chloroethyl) Ether < 660 660 541-73-1 1,3-Dichlorobenzene < 660 660
106-46-7 1,4-Dichlorobenzene < 660 660 95-50-1 1,2-Dichlorobenzene < 660 660
100-51-6 Benzyl Alcohol < 660 660 bis (2-chloroisopropyl)
Ether
108-60-1 < 660 660
95-48-7 2-Methylphenol (O-Cresol) < 660 660 621-64-7 N-Nitroso-di-n-propylamine < 660 660
67-72-1 Hexachloroethane < 660 660 3 & 4-Methylphenol (M &P-
Cresol)
< 660 660
88-75-5 2-Nitrophenol < 660 660 91-20-3 Naphthalene < 660 660
98-95-3 Nitrobenzene < 660 660 78-59-1 Isophorone < 660 660
105-67-9 2,4-Dimethylphenol < 660 660 bis(-2-
Chloroethoxy)Methane
111-91-1 < 660 660
120-83-2 2,4-Dichlorophenol < 660 660 120-82-1 1,2,4-Trichlorobenzene < 660 660
106-47-8 4-Chloroaniline < 660 660 91-57-6 2-Methylnaphthalene < 660 660
77-47-4 Hexachlorocyclopentadiene < 660 660 88-06-2 2,4,6-Trichlorophenol < 660 660
95-95-4 2,4,5-Trichlorophenol < 660 660 91-58-7 2-Chloronaphthalene < 660 660
88-74-4 2-Nitroaniline < 660 660 131-11-13 Dimethyl phthalate < 660 660
51-28-5 2,4-Dinitrophenol < 660 660 606-20-2 2,6-Dinitrotoluene < 660 660
99-09-2 3-Nitroaniline < 3300 3300 132-64-9 Dibenzofuran < 660 660
100-02-7 4-Nitrophenol < 660 660 121-14-2 2,4-Dinitrotoluene < 660 660
100-01-6 4-Nitroaniline < 3300 3300 84-66-2 Diethylphthalate < 660 660
7005-72-3 4-Chlorophenyl-phenylether < 660 660 208-96-8 Acenaphthylene < 660 660
83-32-9 Acenaphthene < 660 660 86-73-7 Fluorene < 660 660
87-86-5 Pentachlorophenol < 3300 3300 86-30-6 N-Nitrosodiphenylamine < 660 660
101-55-3 4-Bromophenyl-phenylether < 660 660 118-74-1 Hexachlorobenzene < 660 660
84-74-2 Di-n-Butylphthalate < 660 660 85-01-8 Phenanthrene < 660 660
120-12-7 Anthracene < 660 660 206-44-0 Fluoranthene < 660 660
The results contained in this report
Page 19 of 43 relate only to those items tested.
Page 29 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
Laboratory ID: A5091-10
Sample ID: SS-10 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
µg/Kg µg/Kg µg/Kg µg/Kg
85-68-7 Butylbenzylphthalate < 660 660 91-94-1 3,3'-Dichlorobenzidine < 660 660
129-00-0 Pyrene < 660 660 117-81-7 bis (2-Ethylhexyl) Phthalate < 660 660
56-55-3 Benzo[a]anthracene < 660 660 218-01-9 Chrysene < 660 660
117-84-0 Di-n-Octylphthalate < 660 660 207-flouranthene08-2 Benzo[b]< 660 660
207-08-9 Benzo[k]fluoranthene < 660 660 50-32-8 Benzo[a]pyrene < 660 660
53-70-3 Dibenzo(a,h)anthracene < 660 660 193-39-5 Indeno (1,2,3-cd) Pyrene < 660 660
191-24-2 Benzo(g,h,i)perylene < 660 660
Compound % Recovery % Rec. Limits
QA/QC SURROGATE RECOVERIES
2-Fluorophenol 97 25-121
Phenol-d5 112 24-133
Nitrobenzene-d5 75 23-120
2,4,6-Tribromophenol 76 19-122
2-Fluorobiphenyl 107 30-115
Terphenyl-d14 105 18-137
TECHNOLOGY LABORATORY, INC.
The results contained in this report
Page 20 of 43 relate only to those items tested.
Page 30 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
11/09/11
11/10/11
Laboratory ID: A5091-11
Sample ID: SB-1 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
11/17/11
Soil
µg/Kg µg/Kg µg/Kg µg/Kg
Sampled:
Received:
Analyzed:
Matrix:
110-86-1 Pyridine < 660 660 62-75-9 N-Nitrosodimethylamine < 660 660
108-95-2 Phenol < 660 660 95-57-8 2-Chlorophenol < 660 660
111-44-4 bis(-2-Chloroethyl) Ether < 660 660 541-73-1 1,3-Dichlorobenzene < 660 660
106-46-7 1,4-Dichlorobenzene < 660 660 95-50-1 1,2-Dichlorobenzene < 660 660
100-51-6 Benzyl Alcohol < 660 660 bis (2-chloroisopropyl)
Ether
108-60-1 < 660 660
95-48-7 2-Methylphenol (O-Cresol) < 660 660 621-64-7 N-Nitroso-di-n-propylamine < 660 660
67-72-1 Hexachloroethane < 660 660 3 & 4-Methylphenol (M &P-
Cresol)
< 660 660
88-75-5 2-Nitrophenol < 660 660 91-20-3 Naphthalene < 660 660
98-95-3 Nitrobenzene < 660 660 78-59-1 Isophorone < 660 660
105-67-9 2,4-Dimethylphenol < 660 660 bis(-2-
Chloroethoxy)Methane
111-91-1 < 660 660
120-83-2 2,4-Dichlorophenol < 660 660 120-82-1 1,2,4-Trichlorobenzene < 660 660
106-47-8 4-Chloroaniline < 660 660 91-57-6 2-Methylnaphthalene < 660 660
77-47-4 Hexachlorocyclopentadiene < 660 660 88-06-2 2,4,6-Trichlorophenol < 660 660
95-95-4 2,4,5-Trichlorophenol < 660 660 91-58-7 2-Chloronaphthalene < 660 660
88-74-4 2-Nitroaniline < 660 660 131-11-13 Dimethyl phthalate < 660 660
51-28-5 2,4-Dinitrophenol < 660 660 606-20-2 2,6-Dinitrotoluene < 660 660
99-09-2 3-Nitroaniline < 3300 3300 132-64-9 Dibenzofuran < 660 660
100-02-7 4-Nitrophenol < 660 660 121-14-2 2,4-Dinitrotoluene < 660 660
100-01-6 4-Nitroaniline < 3300 3300 84-66-2 Diethylphthalate < 660 660
7005-72-3 4-Chlorophenyl-phenylether < 660 660 208-96-8 Acenaphthylene < 660 660
83-32-9 Acenaphthene < 660 660 86-73-7 Fluorene < 660 660
87-86-5 Pentachlorophenol < 3300 3300 86-30-6 N-Nitrosodiphenylamine < 660 660
101-55-3 4-Bromophenyl-phenylether < 660 660 118-74-1 Hexachlorobenzene < 660 660
84-74-2 Di-n-Butylphthalate < 660 660 85-01-8 Phenanthrene < 660 660
120-12-7 Anthracene < 660 660 206-44-0 Fluoranthene < 660 660
The results contained in this report
Page 21 of 43 relate only to those items tested.
Page 31 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
Laboratory ID: A5091-11
Sample ID: SB-1 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
µg/Kg µg/Kg µg/Kg µg/Kg
85-68-7 Butylbenzylphthalate < 660 660 91-94-1 3,3'-Dichlorobenzidine < 660 660
129-00-0 Pyrene < 660 660 117-81-7 bis (2-Ethylhexyl) Phthalate < 660 660
56-55-3 Benzo[a]anthracene < 660 660 218-01-9 Chrysene < 660 660
117-84-0 Di-n-Octylphthalate < 660 660 207-flouranthene08-2 Benzo[b]< 660 660
207-08-9 Benzo[k]fluoranthene < 660 660 50-32-8 Benzo[a]pyrene < 660 660
53-70-3 Dibenzo(a,h)anthracene < 660 660 193-39-5 Indeno (1,2,3-cd) Pyrene < 660 660
191-24-2 Benzo(g,h,i)perylene < 660 660
Compound % Recovery % Rec. Limits
QA/QC SURROGATE RECOVERIES
2-Fluorophenol 85 25-121
Phenol-d5 112 24-133
Nitrobenzene-d5 62 23-120
2,4,6-Tribromophenol 55 19-122
2-Fluorobiphenyl 104 30-115
Terphenyl-d14 116 18-137
TECHNOLOGY LABORATORY, INC.
The results contained in this report
Page 22 of 43 relate only to those items tested.
Page 32 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
11/09/11
11/10/11
Laboratory ID: A5091-12
Sample ID: SB-2 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
11/17/11
Soil
µg/Kg µg/Kg µg/Kg µg/Kg
Sampled:
Received:
Analyzed:
Matrix:
110-86-1 Pyridine < 660 660 62-75-9 N-Nitrosodimethylamine < 660 660
108-95-2 Phenol < 660 660 95-57-8 2-Chlorophenol < 660 660
111-44-4 bis(-2-Chloroethyl) Ether < 660 660 541-73-1 1,3-Dichlorobenzene < 660 660
106-46-7 1,4-Dichlorobenzene < 660 660 95-50-1 1,2-Dichlorobenzene < 660 660
100-51-6 Benzyl Alcohol < 660 660 bis (2-chloroisopropyl)
Ether
108-60-1 < 660 660
95-48-7 2-Methylphenol (O-Cresol) < 660 660 621-64-7 N-Nitroso-di-n-propylamine < 660 660
67-72-1 Hexachloroethane < 660 660 3 & 4-Methylphenol (M &P-
Cresol)
< 660 660
88-75-5 2-Nitrophenol < 660 660 91-20-3 Naphthalene < 660 660
98-95-3 Nitrobenzene < 660 660 78-59-1 Isophorone < 660 660
105-67-9 2,4-Dimethylphenol < 660 660 bis(-2-
Chloroethoxy)Methane
111-91-1 < 660 660
120-83-2 2,4-Dichlorophenol < 660 660 120-82-1 1,2,4-Trichlorobenzene < 660 660
106-47-8 4-Chloroaniline < 660 660 91-57-6 2-Methylnaphthalene < 660 660
77-47-4 Hexachlorocyclopentadiene < 660 660 88-06-2 2,4,6-Trichlorophenol < 660 660
95-95-4 2,4,5-Trichlorophenol < 660 660 91-58-7 2-Chloronaphthalene < 660 660
88-74-4 2-Nitroaniline < 660 660 131-11-13 Dimethyl phthalate < 660 660
51-28-5 2,4-Dinitrophenol < 660 660 606-20-2 2,6-Dinitrotoluene < 660 660
99-09-2 3-Nitroaniline < 3300 3300 132-64-9 Dibenzofuran < 660 660
100-02-7 4-Nitrophenol < 660 660 121-14-2 2,4-Dinitrotoluene < 660 660
100-01-6 4-Nitroaniline < 3300 3300 84-66-2 Diethylphthalate < 660 660
7005-72-3 4-Chlorophenyl-phenylether < 660 660 208-96-8 Acenaphthylene < 660 660
83-32-9 Acenaphthene < 660 660 86-73-7 Fluorene < 660 660
87-86-5 Pentachlorophenol < 3300 3300 86-30-6 N-Nitrosodiphenylamine < 660 660
101-55-3 4-Bromophenyl-phenylether < 660 660 118-74-1 Hexachlorobenzene < 660 660
84-74-2 Di-n-Butylphthalate < 660 660 85-01-8 Phenanthrene < 660 660
120-12-7 Anthracene < 660 660 206-44-0 Fluoranthene < 660 660
The results contained in this report
Page 23 of 43 relate only to those items tested.
Page 33 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
Laboratory ID: A5091-12
Sample ID: SB-2 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
µg/Kg µg/Kg µg/Kg µg/Kg
85-68-7 Butylbenzylphthalate < 660 660 91-94-1 3,3'-Dichlorobenzidine < 660 660
129-00-0 Pyrene < 660 660 117-81-7 bis (2-Ethylhexyl) Phthalate < 660 660
56-55-3 Benzo[a]anthracene < 660 660 218-01-9 Chrysene < 660 660
117-84-0 Di-n-Octylphthalate < 660 660 207-flouranthene08-2 Benzo[b]< 660 660
207-08-9 Benzo[k]fluoranthene < 660 660 50-32-8 Benzo[a]pyrene < 660 660
53-70-3 Dibenzo(a,h)anthracene < 660 660 193-39-5 Indeno (1,2,3-cd) Pyrene < 660 660
191-24-2 Benzo(g,h,i)perylene < 660 660
Compound % Recovery % Rec. Limits
QA/QC SURROGATE RECOVERIES
2-Fluorophenol 86 25-121
Phenol-d5 118 24-133
Nitrobenzene-d5 67 23-120
2,4,6-Tribromophenol 55 19-122
2-Fluorobiphenyl 104 30-115
Terphenyl-d14 117 18-137
TECHNOLOGY LABORATORY, INC.
The results contained in this report
Page 24 of 43 relate only to those items tested.
Page 34 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
11/09/11
11/10/11
Laboratory ID: A5091-13
Sample ID: SB-3 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
11/17/11
Soil
µg/Kg µg/Kg µg/Kg µg/Kg
Sampled:
Received:
Analyzed:
Matrix:
110-86-1 Pyridine < 660 660 62-75-9 N-Nitrosodimethylamine < 660 660
108-95-2 Phenol < 660 660 95-57-8 2-Chlorophenol < 660 660
111-44-4 bis(-2-Chloroethyl) Ether < 660 660 541-73-1 1,3-Dichlorobenzene < 660 660
106-46-7 1,4-Dichlorobenzene < 660 660 95-50-1 1,2-Dichlorobenzene < 660 660
100-51-6 Benzyl Alcohol < 660 660 bis (2-chloroisopropyl)
Ether
108-60-1 < 660 660
95-48-7 2-Methylphenol (O-Cresol) < 660 660 621-64-7 N-Nitroso-di-n-propylamine < 660 660
67-72-1 Hexachloroethane < 660 660 3 & 4-Methylphenol (M &P-
Cresol)
< 660 660
88-75-5 2-Nitrophenol < 660 660 91-20-3 Naphthalene < 660 660
98-95-3 Nitrobenzene < 660 660 78-59-1 Isophorone < 660 660
105-67-9 2,4-Dimethylphenol < 660 660 bis(-2-
Chloroethoxy)Methane
111-91-1 < 660 660
120-83-2 2,4-Dichlorophenol < 660 660 120-82-1 1,2,4-Trichlorobenzene < 660 660
106-47-8 4-Chloroaniline < 660 660 91-57-6 2-Methylnaphthalene < 660 660
77-47-4 Hexachlorocyclopentadiene < 660 660 88-06-2 2,4,6-Trichlorophenol < 660 660
95-95-4 2,4,5-Trichlorophenol < 660 660 91-58-7 2-Chloronaphthalene < 660 660
88-74-4 2-Nitroaniline < 660 660 131-11-13 Dimethyl phthalate < 660 660
51-28-5 2,4-Dinitrophenol < 660 660 606-20-2 2,6-Dinitrotoluene < 660 660
99-09-2 3-Nitroaniline < 3300 3300 132-64-9 Dibenzofuran < 660 660
100-02-7 4-Nitrophenol < 660 660 121-14-2 2,4-Dinitrotoluene < 660 660
100-01-6 4-Nitroaniline < 3300 3300 84-66-2 Diethylphthalate < 660 660
7005-72-3 4-Chlorophenyl-phenylether < 660 660 208-96-8 Acenaphthylene < 660 660
83-32-9 Acenaphthene < 660 660 86-73-7 Fluorene < 660 660
87-86-5 Pentachlorophenol < 3300 3300 86-30-6 N-Nitrosodiphenylamine < 660 660
101-55-3 4-Bromophenyl-phenylether < 660 660 118-74-1 Hexachlorobenzene < 660 660
84-74-2 Di-n-Butylphthalate < 660 660 85-01-8 Phenanthrene < 660 660
120-12-7 Anthracene < 660 660 206-44-0 Fluoranthene < 660 660
The results contained in this report
Page 25 of 43 relate only to those items tested.
Page 35 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
Laboratory ID: A5091-13
Sample ID: SB-3 Project No.: Energy & Engines Co
Method: EPA-8270C
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
µg/Kg µg/Kg µg/Kg µg/Kg
85-68-7 Butylbenzylphthalate < 660 660 91-94-1 3,3'-Dichlorobenzidine < 660 660
129-00-0 Pyrene < 660 660 117-81-7 bis (2-Ethylhexyl) Phthalate < 660 660
56-55-3 Benzo[a]anthracene < 660 660 218-01-9 Chrysene < 660 660
117-84-0 Di-n-Octylphthalate < 660 660 207-flouranthene08-2 Benzo[b]< 660 660
207-08-9 Benzo[k]fluoranthene < 660 660 50-32-8 Benzo[a]pyrene < 660 660
53-70-3 Dibenzo(a,h)anthracene < 660 660 193-39-5 Indeno (1,2,3-cd) Pyrene < 660 660
191-24-2 Benzo(g,h,i)perylene < 660 660
Compound % Recovery % Rec. Limits
QA/QC SURROGATE RECOVERIES
2-Fluorophenol 91 25-121
Phenol-d5 103 24-133
Nitrobenzene-d5 68 23-120
2,4,6-Tribromophenol 47 19-122
2-Fluorobiphenyl 107 30-115
Terphenyl-d14 108 18-137
TECHNOLOGY LABORATORY, INC.
The results contained in this report
Page 26 of 43 relate only to those items tested.
Page 36 of 80
TECHNOLOGY LABORATORY, INC.
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
11/09/11
11/10/11
Laboratory ID: A5091-11
Sample ID: SB-1 Project No.: Energy & Engines Co
Method: EPA-8260B
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
11/15/11
Soil
µg/Kg µg/Kg µg/Kg µg/Kg
Sampled:
Received:
Analyzed:
Matrix:
71-43-2 Benzene < 10 10 108-88-3 Toluene < 10 10
100-41-4 Ethylbenzene < 10 10 1330-20-7 Total Xylenes < 10 10
91-20-3 Naphthalene < 10 10 75-01-4 Vinyl Chloride < 10 10
74-87-3 Chloromethane < 10 10 74-83-9 Bromomethane < 10 10
75-00-3 Chloroethane < 10 10 75-69-4 Trichlorofluoromethane < 10 10
75-35-4 1,1-Dichloroethene < 10 10 156-60-5 trans-1,2-Dichloroethene < 10 10
156-59-2 cis-1,2-Dichloroethene < 10 10 75-09-2 Methylene Chloride < 10 10
75-34-3 1,1-Dichloroethane < 10 10 74-97-5 Bromochloromethane < 10 10
67-66-3 Chloroform < 10 10 71-55-6 1,1,1-Trichloroethane < 10 10
56-23-5 Carbon Tetrachloride < 10 10 107-06-2 1,2-Dichloroethane < 10 10
79-01-6 Trichloroethene < 10 10 78-87-5 1,2-Dichloropropane < 10 10
75-27-4 Bromodichloromethane < 10 10 74-95-3 Dibromomethane < 10 10
79-00-5 1,1,2-Trichloroethane < 10 10 142-28-9 1,3-Dichloropropane < 10 10
590-20-7 2,2-Dichloropropane < 10 10 563-58-6 1,1-Dichloropropene < 10 10
10061-01-5 cis-1,3-Dichloropropene < 10 10 10061-02-6 trans-1,3-Dichloropropene < 10 10
127-18-4 Tetrachloroethene < 10 10 106-93-4 1,2-Dibromoethane (EDB) < 10 10
124-48-1 Dibromochloromethane < 10 10 108-90-7 Chlorobenzene < 10 10
630-20-6 1,1,1,2-Tetrachloroethane < 10 10 100-42-5 Styrene < 10 10
75-25-2 Bromoform < 10 10 79-34-5 1,1,2,2-Tetrachloroethane < 10 10
98-82-8 Isopropylbenzene < 10 10 78-93-3 2-Butanone (MEK) < 10 10
108-86-1 Bromobenzene < 10 10 103-65-1 n-Propylbenzene < 10 10
95-49-8 2-Chlorotoluene < 10 10 106-43-4 4-Chlorotoluene < 10 10
108-67-8 1,3,5-Trimethylbenzene < 10 10 95-63-6 1,2,4-Trimethylbenzene < 10 10
98-06-6 tert-Butylbenzene < 10 10 135-98-8 sec-Butylbenzene < 10 10
541-73-1 1,3-Dichlorobenzene < 10 10 106-46-7 1,4-Dichlorobenzene < 10 10
99-87-6 4-Isopropyltoluene < 10 10 104-51-8 n-Butylbenzene < 10 10
108-10-1 4-Methyl-2-Pentanone (MIBK) < 10 10 120-82-1 1,2,4-Trichlorobenzene < 10 10
87-61-6 1,2,3-Trichlorobenzene < 10 10 87-68-3 Hexachlorobutadiene < 10 10
95-50-1 1,2-Dichlorobenzene < 10 10 67-64-1 Acetone < 100 100
Compound % Recovery % Rec. Limits
QA/QC SURROGATE RECOVERIES
Dibromofluoromethane 110 68-120
Toluene-d8 104 81-128
Bromofluorobenzene 75 70-113
The results contained in this report
relate only to those items tested.
TECHNOLOGY LABORATORY, INC.
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
11/09/11
11/10/11
Laboratory ID: A5091-12
Sample ID: SB-2 Project No.: Energy & Engines Co
Method: EPA-8260B
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
11/15/11
Soil
µg/Kg µg/Kg µg/Kg µg/Kg
Sampled:
Received:
Analyzed:
Matrix:
71-43-2 Benzene < 10 10 108-88-3 Toluene < 10 10
100-41-4 Ethylbenzene < 10 10 1330-20-7 Total Xylenes < 10 10
91-20-3 Naphthalene < 10 10 75-01-4 Vinyl Chloride < 10 10
74-87-3 Chloromethane < 10 10 74-83-9 Bromomethane < 10 10
75-00-3 Chloroethane < 10 10 75-69-4 Trichlorofluoromethane < 10 10
75-35-4 1,1-Dichloroethene < 10 10 156-60-5 trans-1,2-Dichloroethene < 10 10
156-59-2 cis-1,2-Dichloroethene < 10 10 75-09-2 Methylene Chloride < 10 10
75-34-3 1,1-Dichloroethane < 10 10 74-97-5 Bromochloromethane < 10 10
67-66-3 Chloroform < 10 10 71-55-6 1,1,1-Trichloroethane < 10 10
56-23-5 Carbon Tetrachloride < 10 10 107-06-2 1,2-Dichloroethane < 10 10
79-01-6 Trichloroethene < 10 10 78-87-5 1,2-Dichloropropane < 10 10
75-27-4 Bromodichloromethane < 10 10 74-95-3 Dibromomethane < 10 10
79-00-5 1,1,2-Trichloroethane < 10 10 142-28-9 1,3-Dichloropropane < 10 10
590-20-7 2,2-Dichloropropane < 10 10 563-58-6 1,1-Dichloropropene < 10 10
10061-01-5 cis-1,3-Dichloropropene < 10 10 10061-02-6 trans-1,3-Dichloropropene < 10 10
127-18-4 Tetrachloroethene < 10 10 106-93-4 1,2-Dibromoethane (EDB) < 10 10
124-48-1 Dibromochloromethane < 10 10 108-90-7 Chlorobenzene < 10 10
630-20-6 1,1,1,2-Tetrachloroethane < 10 10 100-42-5 Styrene < 10 10
75-25-2 Bromoform < 10 10 79-34-5 1,1,2,2-Tetrachloroethane < 10 10
98-82-8 Isopropylbenzene < 10 10 78-93-3 2-Butanone (MEK) < 10 10
108-86-1 Bromobenzene < 10 10 103-65-1 n-Propylbenzene < 10 10
95-49-8 2-Chlorotoluene < 10 10 106-43-4 4-Chlorotoluene < 10 10
108-67-8 1,3,5-Trimethylbenzene < 10 10 95-63-6 1,2,4-Trimethylbenzene < 10 10
98-06-6 tert-Butylbenzene < 10 10 135-98-8 sec-Butylbenzene < 10 10
541-73-1 1,3-Dichlorobenzene < 10 10 106-46-7 1,4-Dichlorobenzene < 10 10
99-87-6 4-Isopropyltoluene < 10 10 104-51-8 n-Butylbenzene < 10 10
108-10-1 4-Methyl-2-Pentanone (MIBK) < 10 10 120-82-1 1,2,4-Trichlorobenzene < 10 10
87-61-6 1,2,3-Trichlorobenzene < 10 10 87-68-3 Hexachlorobutadiene < 10 10
95-50-1 1,2-Dichlorobenzene < 10 10 67-64-1 Acetone < 100 100
Compound % Recovery % Rec. Limits
QA/QC SURROGATE RECOVERIES
Dibromofluoromethane 105 68-120
Toluene-d8 99 81-128
Bromofluorobenzene 80 70-113
The results contained in this report
relate only to those items tested.
TECHNOLOGY LABORATORY, INC.
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
11/09/11
11/10/11
Laboratory ID: A5091-13
Sample ID: SB-3 Project No.: Energy & Engines Co
Method: EPA-8260B
Number Parameter
CAS Result MDL
Number Parameter
CAS Result MDL
11/15/11
Soil
µg/Kg µg/Kg µg/Kg µg/Kg
Sampled:
Received:
Analyzed:
Matrix:
71-43-2 Benzene < 10 10 108-88-3 Toluene 14.6 10
100-41-4 Ethylbenzene < 10 10 1330-20-7 Total Xylenes < 10 10
91-20-3 Naphthalene < 10 10 75-01-4 Vinyl Chloride < 10 10
74-87-3 Chloromethane < 10 10 74-83-9 Bromomethane < 10 10
75-00-3 Chloroethane < 10 10 75-69-4 Trichlorofluoromethane < 10 10
75-35-4 1,1-Dichloroethene < 10 10 156-60-5 trans-1,2-Dichloroethene < 10 10
156-59-2 cis-1,2-Dichloroethene < 10 10 75-09-2 Methylene Chloride < 10 10
75-34-3 1,1-Dichloroethane < 10 10 74-97-5 Bromochloromethane < 10 10
67-66-3 Chloroform < 10 10 71-55-6 1,1,1-Trichloroethane < 10 10
56-23-5 Carbon Tetrachloride < 10 10 107-06-2 1,2-Dichloroethane < 10 10
79-01-6 Trichloroethene < 10 10 78-87-5 1,2-Dichloropropane < 10 10
75-27-4 Bromodichloromethane < 10 10 74-95-3 Dibromomethane < 10 10
79-00-5 1,1,2-Trichloroethane < 10 10 142-28-9 1,3-Dichloropropane < 10 10
590-20-7 2,2-Dichloropropane < 10 10 563-58-6 1,1-Dichloropropene < 10 10
10061-01-5 cis-1,3-Dichloropropene < 10 10 10061-02-6 trans-1,3-Dichloropropene < 10 10
127-18-4 Tetrachloroethene < 10 10 106-93-4 1,2-Dibromoethane (EDB) < 10 10
124-48-1 Dibromochloromethane < 10 10 108-90-7 Chlorobenzene < 10 10
630-20-6 1,1,1,2-Tetrachloroethane < 10 10 100-42-5 Styrene < 10 10
75-25-2 Bromoform < 10 10 79-34-5 1,1,2,2-Tetrachloroethane < 10 10
98-82-8 Isopropylbenzene < 10 10 78-93-3 2-Butanone (MEK) < 10 10
108-86-1 Bromobenzene < 10 10 103-65-1 n-Propylbenzene < 10 10
95-49-8 2-Chlorotoluene < 10 10 106-43-4 4-Chlorotoluene < 10 10
108-67-8 1,3,5-Trimethylbenzene < 10 10 95-63-6 1,2,4-Trimethylbenzene < 10 10
98-06-6 tert-Butylbenzene < 10 10 135-98-8 sec-Butylbenzene < 10 10
541-73-1 1,3-Dichlorobenzene < 10 10 106-46-7 1,4-Dichlorobenzene < 10 10
99-87-6 4-Isopropyltoluene < 10 10 104-51-8 n-Butylbenzene < 10 10
108-10-1 4-Methyl-2-Pentanone (MIBK) < 10 10 120-82-1 1,2,4-Trichlorobenzene < 10 10
87-61-6 1,2,3-Trichlorobenzene < 10 10 87-68-3 Hexachlorobutadiene < 10 10
95-50-1 1,2-Dichlorobenzene < 10 10 67-64-1 Acetone < 100 100
Compound % Recovery % Rec. Limits
QA/QC SURROGATE RECOVERIES
Dibromofluoromethane 107 68-120
Toluene-d8 102 81-128
Bromofluorobenzene 77 70-113
The results contained in this report
relate only to those items tested.
! !
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL OFFICE PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services Date Received: 11/10/2011
1136 East Stuart, Suite 4204 Matrix: Soil
Fort Collins, CO 80525 Project No.: Energy & Engines
Conversion Lab
Method: EPA-7061A
Date Date Arsenic
Lab ID Sample ID Sampled Analyzed mg/kg
A5091-01 SS-1 11/09/11 11/23/11 0.506
A5091-02 SS-2 11/09/11 11/23/11 0.333
A5091-03 SS-3 11/09/11 11/23/11 0.489
A5091-04 SS-4 11/09/11 11/23/11 0.295
A5091-05 SS-5 11/09/11 11/23/11 0.398
A5091-06 SS-6 11/09/11 11/23/11 0.432
A5091-07 SS-7 11/09/11 11/23/11 0.395
A5091-08 SS-8 11/09/11 11/23/11 2.14
A5091-09 SS-9 11/09/11 11/23/11 0.779
A5091-10 SS-10 11/09/11 11/23/11 1.04
A5091-11 SB-1 11/09/11 11/23/11 0.815
A5091-12 SB-2 11/09/11 11/23/11 0.769
A5091-13 SB-3 11/09/11 11/23/11 0.861
Page 30 of 43
Page 40 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
Sampled: 11/09/11
Received: 11/10/11
Laboratory ID A5091-01
Sample ID: SS-1 Project No.: Energy & Engines
Conversion Lab
Matrix: Soil
Number Parameter Result Units Method Analyzed
CAS Date
MDL
7440-39-3 Total Barium 113 mg/Kg 0.25 EPA-6010B 11/23/11
7440-43-9 Total Cadmium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7440-47-3 Total Chromium 13.5 mg/Kg 0.25 EPA-6010B 11/23/11
7439-92-1 Total Lead 26.5 mg/Kg 0.15 EPA-6010B 11/23/11
7782-49-2 Total Selenium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7740-22-4 Total Silver < 0.30 mg/Kg 0.3 EPA-6010B 11/23/11
7439-97-6 Total Mercury < 0.25 mg/Kg 0.25 EPA-7470A 11/21/11
The results contained in this report
relate only to those items tested.
Page 31 of 43
Page 41 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
Sampled: 11/09/11
Received: 11/10/11
Laboratory ID A5091-02
Sample ID: SS-2 Project No.: Energy & Engines
Conversion Lab
Matrix: Soil
Number Parameter Result Units Method Analyzed
CAS Date
MDL
7440-39-3 Total Barium 144 mg/Kg 0.25 EPA-6010B 11/23/11
7440-43-9 Total Cadmium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7440-47-3 Total Chromium 14.1 mg/Kg 0.25 EPA-6010B 11/23/11
7439-92-1 Total Lead 34.0 mg/Kg 0.15 EPA-6010B 11/23/11
7782-49-2 Total Selenium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7740-22-4 Total Silver < 0.30 mg/Kg 0.3 EPA-6010B 11/23/11
7439-97-6 Total Mercury < 0.25 mg/Kg 0.25 EPA-7470A 11/21/11
The results contained in this report
relate only to those items tested.
Page 32 of 43
Page 42 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
Sampled: 11/09/11
Received: 11/10/11
Laboratory ID A5091-03
Sample ID: SS-3 Project No.: Energy & Engines
Conversion Lab
Matrix: Soil
Number Parameter Result Units Method Analyzed
CAS Date
MDL
7440-39-3 Total Barium 115 mg/Kg 0.25 EPA-6010B 11/23/11
7440-43-9 Total Cadmium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7440-47-3 Total Chromium 12.9 mg/Kg 0.25 EPA-6010B 11/23/11
7439-92-1 Total Lead 21.0 mg/Kg 0.15 EPA-6010B 11/23/11
7782-49-2 Total Selenium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7740-22-4 Total Silver < 0.30 mg/Kg 0.3 EPA-6010B 11/23/11
7439-97-6 Total Mercury < 0.25 mg/Kg 0.25 EPA-7470A 11/21/11
The results contained in this report
relate only to those items tested.
Page 33 of 43
Page 43 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
Sampled: 11/09/11
Received: 11/10/11
Laboratory ID A5091-04
Sample ID: SS-4 Project No.: Energy & Engines
Conversion Lab
Matrix: Soil
Number Parameter Result Units Method Analyzed
CAS Date
MDL
7440-39-3 Total Barium 88.3 mg/Kg 0.25 EPA-6010B 11/23/11
7440-43-9 Total Cadmium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7440-47-3 Total Chromium 11.6 mg/Kg 0.25 EPA-6010B 11/23/11
7439-92-1 Total Lead 28.1 mg/Kg 0.15 EPA-6010B 11/23/11
7782-49-2 Total Selenium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7740-22-4 Total Silver < 0.30 mg/Kg 0.3 EPA-6010B 11/23/11
7439-97-6 Total Mercury < 0.25 mg/Kg 0.25 EPA-7470A 11/21/11
The results contained in this report
relate only to those items tested.
Page 34 of 43
Page 44 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
Sampled: 11/09/11
Received: 11/10/11
Laboratory ID A5091-05
Sample ID: SS-5 Project No.: Energy & Engines
Conversion Lab
Matrix: Soil
Number Parameter Result Units Method Analyzed
CAS Date
MDL
7440-39-3 Total Barium 135 mg/Kg 0.25 EPA-6010B 11/23/11
7440-43-9 Total Cadmium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7440-47-3 Total Chromium 13.8 mg/Kg 0.25 EPA-6010B 11/23/11
7439-92-1 Total Lead 19.6 mg/Kg 0.15 EPA-6010B 11/23/11
7782-49-2 Total Selenium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7740-22-4 Total Silver < 0.30 mg/Kg 0.3 EPA-6010B 11/23/11
7439-97-6 Total Mercury < 0.25 mg/Kg 0.25 EPA-7470A 11/21/11
The results contained in this report
relate only to those items tested.
Page 35 of 43
Page 45 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
Sampled: 11/09/11
Received: 11/10/11
Laboratory ID A5091-06
Sample ID: SS-6 Project No.: Energy & Engines
Conversion Lab
Matrix: Soil
Number Parameter Result Units Method Analyzed
CAS Date
MDL
7440-39-3 Total Barium 394 mg/Kg 0.25 EPA-6010B 11/23/11
7440-43-9 Total Cadmium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7440-47-3 Total Chromium 8.40 mg/Kg 0.25 EPA-6010B 11/23/11
7439-92-1 Total Lead 126 mg/Kg 0.15 EPA-6010B 11/23/11
7782-49-2 Total Selenium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7740-22-4 Total Silver < 0.30 mg/Kg 0.3 EPA-6010B 11/23/11
7439-97-6 Total Mercury < 0.25 mg/Kg 0.25 EPA-7470A 11/21/11
The results contained in this report
relate only to those items tested.
Page 36 of 43
Page 46 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
Sampled: 11/09/11
Received: 11/10/11
Laboratory ID A5091-07
Sample ID: SS-7 Project No.: Energy & Engines
Conversion Lab
Matrix: Soil
Number Parameter Result Units Method Analyzed
CAS Date
MDL
7440-39-3 Total Barium 115 mg/Kg 0.25 EPA-6010B 11/23/11
7440-43-9 Total Cadmium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7440-47-3 Total Chromium 10.6 mg/Kg 0.25 EPA-6010B 11/23/11
7439-92-1 Total Lead 80.7 mg/Kg 0.15 EPA-6010B 11/23/11
7782-49-2 Total Selenium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7740-22-4 Total Silver < 0.30 mg/Kg 0.3 EPA-6010B 11/23/11
7439-97-6 Total Mercury < 0.25 mg/Kg 0.25 EPA-7470A 11/21/11
The results contained in this report
relate only to those items tested.
Page 37 of 43
Page 47 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
Sampled: 11/09/11
Received: 11/10/11
Laboratory ID A5091-08
Sample ID: SS-8 Project No.: Energy & Engines
Conversion Lab
Matrix: Soil
Number Parameter Result Units Method Analyzed
CAS Date
MDL
7440-39-3 Total Barium 336 mg/Kg 0.25 EPA-6010B 11/23/11
7440-43-9 Total Cadmium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7440-47-3 Total Chromium 11.0 mg/Kg 0.25 EPA-6010B 11/23/11
7439-92-1 Total Lead 499 mg/Kg 0.15 EPA-6010B 11/23/11
7782-49-2 Total Selenium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7740-22-4 Total Silver < 0.30 mg/Kg 0.3 EPA-6010B 11/23/11
7439-97-6 Total Mercury < 0.25 mg/Kg 0.25 EPA-7470A 11/21/11
The results contained in this report
relate only to those items tested.
Page 38 of 43
Page 48 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
Sampled: 11/09/11
Received: 11/10/11
Laboratory ID A5091-09
Sample ID: SS-9 Project No.: Energy & Engines
Conversion Lab
Matrix: Soil
Number Parameter Result Units Method Analyzed
CAS Date
MDL
7440-39-3 Total Barium 482 mg/Kg 0.25 EPA-6010B 11/23/11
7440-43-9 Total Cadmium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7440-47-3 Total Chromium 14.9 mg/Kg 0.25 EPA-6010B 11/23/11
7439-92-1 Total Lead 296 mg/Kg 0.15 EPA-6010B 11/23/11
7782-49-2 Total Selenium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7740-22-4 Total Silver < 0.30 mg/Kg 0.3 EPA-6010B 11/23/11
7439-97-6 Total Mercury 0.27 mg/Kg 0.25 EPA-7470A 11/21/11
The results contained in this report
relate only to those items tested.
Page 39 of 43
Page 49 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
Sampled: 11/09/11
Received: 11/10/11
Laboratory ID A5091-10
Sample ID: SS-10 Project No.: Energy & Engines
Conversion Lab
Matrix: Soil
Number Parameter Result Units Method Analyzed
CAS Date
MDL
7440-39-3 Total Barium 451 mg/Kg 0.25 EPA-6010B 11/23/11
7440-43-9 Total Cadmium 2.00 mg/Kg 0.25 EPA-6010B 11/23/11
7440-47-3 Total Chromium 10.9 mg/Kg 0.25 EPA-6010B 11/23/11
7439-92-1 Total Lead 850 mg/Kg 0.15 EPA-6010B 11/23/11
7782-49-2 Total Selenium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7740-22-4 Total Silver < 0.30 mg/Kg 0.3 EPA-6010B 11/23/11
7439-97-6 Total Mercury < 0.25 mg/Kg 0.25 EPA-7470A 11/21/11
The results contained in this report
relate only to those items tested.
Page 40 of 43
Page 50 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
Sampled: 11/09/11
Received: 11/10/11
Laboratory ID A5091-11
Sample ID: SB-1 Project No.: Energy & Engines
Conversion Lab
Matrix: Soil
Number Parameter Result Units Method Analyzed
CAS Date
MDL
7440-39-3 Total Barium 301 mg/Kg 0.25 EPA-6010B 11/23/11
7440-43-9 Total Cadmium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7440-47-3 Total Chromium 14.9 mg/Kg 0.25 EPA-6010B 11/23/11
7439-92-1 Total Lead 662 mg/Kg 0.15 EPA-6010B 11/23/11
7782-49-2 Total Selenium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7740-22-4 Total Silver < 0.30 mg/Kg 0.3 EPA-6010B 11/23/11
7439-97-6 Total Mercury < 0.25 mg/Kg 0.25 EPA-7470A 11/21/11
The results contained in this report
relate only to those items tested.
Page 41 of 43
Page 51 of 80
TECHNOLOGY LABORATORY, INC.
CENTRE PROFESSIONAL PARK
1012 Centre Avenue
Fort Collins, Colorado 80526
(970) 490-1414
CERTIFICATE OF ANALYSIS
National Inspection Services
1136 East Stuart, Suite 4204
Fort Collins, CO 80525
Sampled: 11/09/11
Received: 11/10/11
Laboratory ID A5091-13
Sample ID: SB-3 Project No.: Energy & Engines
Conversion Lab
Matrix: Soil
Number Parameter Result Units Method Analyzed
CAS Date
MDL
7440-39-3 Total Barium 974 mg/Kg 0.25 EPA-6010B 11/23/11
7440-43-9 Total Cadmium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7440-47-3 Total Chromium 17.9 mg/Kg 0.25 EPA-6010B 11/23/11
7439-92-1 Total Lead 219 mg/Kg 0.15 EPA-6010B 11/23/11
7782-49-2 Total Selenium < 0.25 mg/Kg 0.25 EPA-6010B 11/23/11
7740-22-4 Total Silver < 0.30 mg/Kg 0.3 EPA-6010B 11/23/11
7439-97-6 Total Mercury < 0.25 mg/Kg 0.25 EPA-7470A 11/21/11
The results contained in this report
relate only to those items tested.
Page 43 of 43
Page 53 of 80
Page 54 of 80
Page 1 of 2
Laboratory Code: RES
Subcontract Number: NA
Laboratory Report: RES 224096-1
Project # / P.O. # None Given
Project Description:
RES 224096-1
Sincerely,
Anita Grigg Robert R. Workman Jr.
Bethany Nichols Anya Angst
Reservoirs Environmental, Inc. is an analytical laboratory accredited for the analysis of Industrial Hygiene
and Environmental matrices by the National Voluntary Laboratory Accreditation Program (NVLAP), Lab
Code 101896-0 for Transmission Electron Microscopy (TEM) and Polarized Light Microscopy (PLM)
analysis and the American Industrial Hygiene Association (AIHA), Lab ID 101533 - Accreditation Certificate
#480 for Phase Contrast Microscopy (PCM) analysis. This laboratory is currently proficient in both
Proficiency Testing and PAT programs respectively.
Reservoirs Environmental, Inc. has analyzed the following samples for asbestos content as per your
request. The analysis has been completed in general accordance with the appropriate methodology as
stated in the attached analysis table. The results have been submitted to your office.
National Inspection Svs (Commercial)
1136 E Stuart St Suite 4204
Ft. Collins CO 80525-1193
Energy and Engines
Conversion Lab - 430 N.
College Ave, Fort Collins
November 17, 2011
Analyst(s): _________________________
Paul D. LoScalzo Wenlong Liu
Michael Scales Adam Humphreys
is the job number assigned to this study. This report is considered highly confidential
and the sole property of the customer. Reservoirs Environmental, Inc. will not discuss any part of this study
with personnel other than those of the client. The results described in this report only apply to the samples
analyzed. This report must not be used to claim endorsement of products or analytical results by NVLAP or
any agency of the U.S. Government. This report shall not be reproduced except in full, without written
approval from Reservoirs Environmental, Inc. Samples will be disposed of after sixty days unless longer
storage is requested. If you have any questions about this report, please feel free to call 303-964-1986.
Jeanne Spencer Orr
President
Dear Customer,
P: 303-964-1986
F: 303-477-4275
5801 Logan Street, Suite 100 Denver, CO 80216
Page 1 of 2
1-866-RESI-ENV
www.reilab.com
Page 55 of 80
Page 2 of 2
TABLE PLM BULK ANALYSIS, PERCENTAGE COMPOSITION BY VOLUME
RES Job Number:
Client:
Client Project Number / P.O.:
Client Project Description:
Date Samples Received:
Analysis Type:
Turnaround:
Date Analyzed:
Client Non Non-
Sample Sub Asbestos Fibrous
Number Physical Part Fibrous Components
Description (%) Mineral Visual Components (%)
Estimate (%) (%)
.
SB-1 EM 823327 A Brown soil 100 Chrysotile TR TR 100
SB-2 EM 823328 A Brown soil 100 ND TR 100
SB-3 EM 823329 A Brown soil 100 Chrysotile TR TR 100
SS-1 EM 823330 A Brown soil 100 ND TR 100
SS-2 EM 823331 A Brown soil 100 ND TR 100
SS-3 EM 823332 A Brown soil 100 ND TR 100
SS-4 EM 823333 A Brown soil 100 ND TR 100
SS-5 EM 823334 A Brown soil 100 Chrysotile TR TR 100
SS-6 EM 823335 A Brown soil 100 ND TR 100
SS-7 EM 823336 A Brown soil 100 ND TR 100
SS-8 EM 823337 A Brown soil 100 Chrysotile TR TR 100
SS-9 EM 823338 A Brown soil 100 Chrysotile TR TR 100
SS-10 EM 823339 A Brown soil 100 ND TR 100
Asbestos Content
RES 224096-1
November 14, 2011
None Given
Energy and Engines Conversion Lab - 430 N. College Ave, Fort Collins
National Inspection Svs (Commercial)
November 10, 2011
RESERVOIRS ENVIRONMENTAL, INC.
NVLAP Lab Code 101896-0
TDH Licensed Laboratory # 30-0136
ID Number
L
A
Y
E
R
Lab
PLM, Short Report
3-5 Day
ND=None Detected
TR=Trace, <1% Visual Estimate
Trem-Act=Tremolite-Actinolite
Note: Further analysis by TEM is recommended for organically bound material (i.e. floor tile)
if PLM results are <1%.
_______
Data QA
Page 56 of 80
Page 57 of 80
Phase
II
Subsurface
Investigation
–
430
North
College
Avenue,
Fort
Collins,
Colorado
80524
December
5,
2011
CDPHE
NOTIFICATION
LETTER
Page 58 of 80
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Page 59 of 80
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Page 60 of 80
Century Environmental Hygiene LLC
3201 E. Mulberry St, Unit C, Fort Collins CO 80524
(970) 266-8000 (970) 266-0022 (Fax) www.centuryenvironmental.com
November 10, 2011
National Inspection Service
Mr. Bill Warren
1136 E. Stuart Street, STE 4204
Fort Collins, CO 80525
Re: Asbestos Air Testing @ CSU Power Plant, 430 N College, Fort Collins, CO
CEH Project No.: 3459.11
Dear Mr. Warren:
At your request, Dave Turney, a Colorado licensed Air Monitoring Specialist (CDPHE # 16724),
of Century Environmental Hygiene, LLC (CEH) collected air samples on November 9th, 2011 on
three workers performing potholing work at the project site. The samples were collected for a
three hour period, during the time in which the potholing activity was performed.
Sample Location Sample Number Result
Personal sampling, Ben Schnacker,
point of operation
110911DT-01 0.006 Fibers/cc
Personal sampling, David Valance,
assistance/labor
110911DT-02 0.011 Fibers/cc; sampled sent
in for TEM analysis = 27.3
structures/mm2
Personal sampling, Cleave Berdzar,
Inspector
110911DT-03 0.004 Fibers/cc
Sample 110911DT-01 and -03 were analyzed and contained <0.01 fibers/cc, which was less than
the Colorado Maximum Allowable Asbestos Level (MAAL) of 0.01 fibers/cc. The second
sample 110911DT-02 was analyzed and contained 0.011 fibers/cc, which is over the MAAL.
This sample was sent into Reservoirs Environmental for cross analysis via TEM.
The samples were subsequently analyzed following the analytical aspects of NIOSH 7400, using
optical microscopy (phase contrast microscopy (PCM)) by a CEH analyst. The PCM method
detects all fiber types and does not differentiate between fibers, provided they meet the size and
shape definitions. Thus, the result is a total fiber count, inclusive of asbestos, fiberglass,
cellulose and other fiber-like particles, so the count does not imply asbestos was necessarily
present. The CEH laboratory is currently and historically proficient in the American Industrial
Hygiene Association’s Proficiency Analytical Testing Program for PCM analysis and meets the
requirements of 763.90 (i)(2)(ii).
If you have any questions, please let me know.
Page 61 of 80
Attachments: Air Monitoring Data Sheet, Lab report
Disclaimer:
No evaluations beyond those described in the report have been made and CEH is not responsible for any hazards or
risks, apparent or otherwise, other than those included in this evaluation. As with any conclusions made based on
visual observations and/or random and limited sampling, there is an inherent possibility that undetected conditions
exist, and CEH does not accept liability for any not reasonably ascertainable from the data or observations made.
Sampling can be inherently obtrusive, and CEH does not accept liability for any damage to the property reasonably
occurring during the course of the work in connection with its duties. The only warrantee expressed or implied is
that the work conforms to standard industry practice at the time it was performed. In the unlikely event a defect in
the work is noted, the client has the option to request that the defect be remedied at no additional cost, or a pro rata
deduction in the fee billed. CEH’s maximum liability to any party shall not exceed the fee for the defective portion
of the work. Any reports issued are for the sole use of the client and reliance on it by others it at their sole risk.
Page 62 of 80
Page 63 of 80
Page 1 of 3
Laboratory Code: RES
Subcontract Number: NA
Laboratory Report: RES 224017-1
Project # / P.O. # 3459.11
Project Description:
Jim Dennison
RES 224017-1
Sincerely,
November 10, 2011
is the job number assigned to this study. This report is considered highly confidential
and the sole property of the customer. Reservoirs Environmental, Inc. will not discuss any part of this study
with personnel other than those of the client. The results described in this report only apply to the samples
analyzed. This report must not be used to claim endorsement of products or analytical results by NVLAP or
any agency of the U.S. Government. This report shall not be reproduced except in full, without written
approval from Reservoirs Environmental, Inc. Samples will be disposed of after sixty days unless longer
storage is requested. If you have any questions about this report, please feel free to call 303-964-1986.
Jeanne Spencer Orr
President
Dear Customer,
Reservoirs Environmental, Inc. is an analytical laboratory accredited for the analysis of Industrial Hygiene
and Environmental matrices by the National Voluntary Laboratory Accreditation Program (NVLAP), Lab
Code 101896-0 for Transmission Electron Microscopy (TEM) and Polarized Light Microscopy (PLM)
analysis and the American Industrial Hygiene Association (AIHA), Lab ID 101533 - Accreditation Certificate
#480 for Phase Contrast Microscopy (PCM) analysis. This laboratory is currently proficient in both
Proficiency Testing and PAT programs respectively.
Reservoirs Environmental, Inc. has analyzed the following samples for asbestos content as per your
request. The analysis has been completed in general accordance with the appropriate methodology as
stated in the attached analysis table. The results have been submitted to your office.
Century Environmental Hygiene, LLC
3201 E. Mulberry St. Unit C
Fort Collins CO 80524
430 N. College Ave., FTC
P: 303-964-1986
F: 303-477-4275
5801 Logan Street, Suite 100 Denver, CO 80216
Page 1 of 3
1-866-RESI-ENV
www.reilab.com
Page 64 of 80
RESERVOIRS ENVIRONMENTAL, INC.
NVLAP Lab Code 101896-0; TDH: #30-0015
TABLE I. TEM AIR FILTER SAMPLE DATA AND ANALYTICAL RESULTS
RES Job Number:
Client:
Client Project Number / P.O.:
Client Project Description:
Date Samples Received:
Analysis Type:
Turnaround:
Date Samples Analyzed:
Client Lab Area Air Number of Analytical Asbestos Filter
ID Number ID Number Analyzed Volume Asbestos Sensitivity Concentration Loading
Sampled Structures
Detected
(mm
2
) (L) (s/cc) (s/cc) (s/mm
2
)
110911DT-02 EM 822760 0.1100 512 3 0.0068 0.0205 27.3
NA = Not Analyzed Filter Material = Mixed Cellulose Ester
ND = None Detected Filter Diameter = 25 mm
BAS = Below Analytical Sensitivity Effective Filter Area = 385 sq mm
Average Grid Opening in mm
2
= 0.011
DATA QA
November 10, 2011
RES 224017-1
3459.11
430 N. College Ave., FTC
TEM, LEVEL II
6 Hour
Century Environmental Hygiene, LLC
November 9, 2011
Page 2 of 3
Page 65 of 80
RESERVOIRS ENVIRONMENTAL, INC.
NVLAP Lab Code 101896-0; TDH: #30-0015
TABLE II. SUMMARY OF ANALYTICAL DATA
RES Job Number:
Client:
Client Project Number / P.O.:
Client Project Description:
Date Samples Received:
Analysis Type:
Turnaround:
Date Samples Analyzed:
Client Lab Asbestos Structures **Excluded Asbestos
ID Number ID Number Mineral >5 Microns Structures Structures
Asbestos Structure Types* in Length for
Fibers Bundles Clusters Matrices Concentration
110911DT-02 EM 822760 Chrysotile 2 0 0 1 0 0 3
*See Analytical Procedure for definitions
**C = Excluded from total due to lack of confirmation
**L = Excluded from total for length less than 0.5 micron (AHERA only)
**A = Excluded from total due to incorrect aspect ratio
ND = None Detected
November 10, 2011
RES 224017-1
Century Environmental Hygiene, LLC
6 Hour
TEM, LEVEL II
3459.11
430 N. College Ave., FTC
November 9, 2011
Page 3 of 3
Page 66 of 80
Page 67 of 80
File: Shared on server T/Offforms.sg/Attachment I
Revised: 12/9/10
Attachment I
Key to Count Sheets
Count Sheets
Analytical Procedures
Structures identifications consist of an Asbestos Type followed by a Structure Type
Asbestos Type Structure Types
A = Amosite F = Fiber
An = Anthophyllite B = Bundle
C = Chrysotile C = Cluster
Cr = Crocidolite M = Matrix
T = Tremolite
ND = no structures detected
M = other structure associated with a matrix
NAM = Non Asbestos Mineral
XGB = partly obscured by a grid bar
Sizing Conversion
1 length unit = 5 mm on screen = 0.278 micron
1.80 length units = 0.5 micron
18.0 length units = 5 microns
1 width unit = 1 mm on screen = 0.0556 micron
TEM Analysts
Jeanne S. Orr Paul D. LoScalzo
Nathan DelHierro Mark Steiner
Angela Heitger Norberto Zimbleman
Jonathan Bernard Robert Workman
TEM Confidence Limits
0
5
10
15
20
25
30
35
05101520 Number of Structures Counted
95% Confidence Bounds for No. of
Structures
Upper and lower 95% confidence bounds for the number of structures counted assuming a Poisson distribution.
Page 68 of 80
Page 69 of 80
Page 70 of 80
T:\Office Forms\Level II Attachement.doc
Revised: 3/11/11
Analytical Procedures
Transmission electron microscopy/energy dispersive X-ray spectrometry / selected area
electron diffraction (TEM /EDX / SAED) was employed in the analysis of the sample.
The water was homogenized in an ultrasonic bath and an aliquot was drawn. The aliquot
was diluted as needed (indicated by screening) and an aliquot of the diluted sample was
then drawn through a 0.22 micron pore size mixed cellulose ester filter. A portion of the
filter was collapsed, etched, and then coated with a thin layer of carbon in a carbon
evaporator. A small piece of the coated filter was placed onto a 3mm diameter copper
TEM grid with the carbon side down. The sample was then placed inside a condensation
washer and treated with acetone to remove the filter matrix and expose and inert material.
For each sample, ten grid openings on a 200 mesh TEM grid are searched for fibrous
structures which, if present, are analyzed by SAED and EDX (elemental analysis). Level
II protocol requires SAED confirmation of all asbestos identifications. EDX confirmation
is also required for the first 5 chrysotile structures, the first 10 amphibole structures and
every tenth structure after the 5 or 10 structure minimum is met. The morphology of each
structure is determined and the length and diameter of any asbestos structures is recorded.
Asbestos fibers, bundles, clusters and matrices were identified and recorded. These
asbestos structures have been defined in Yamate et al., as follows:
Fiber: is a structure having an aspect ratio of 3:1 or greater with substantially parallel
sides.
Bundle: is a structure composed of three or more fibers in a parallel arrangement, with
each fiber closer than the diameter of one fiber.
Cluster: is a structure with fibers in a random arrangement such that all fibers are
intermixed and no single fiber is isolated from the group.
Matrix: is a fiber or fibers with one end free and the other end embedded or hidden by a
particulate.
If more than 100 asbestos structures are identified and confirmed on a sample, Level II
analysis may be terminated after completion of the grid opening which contains the 100th
structure.
Equations Used for Calculations
TEM GO Counted
Asbestos Structures
#
#
x ( 2 )
. ( 2 )
AverageTEM GOArea mm
Eff FilterArea mm
x OriginalDi tution / DilutionFa ctors
1
x L
ml
1
1000
GO = TEM Grid Opening
Page 71 of 80
Phase
II
Subsurface
Investigation
–
430
North
College
Avenue,
Fort
Collins,
Colorado
80524
December
5,
2011
STATEMENT
OF
QUALIFICATIONS
Page 72 of 80
Phase
II
Subsurface
Investigation
–
430
North
College
Avenue,
Fort
Collins,
Colorado
80524
December
5,
2011
National
Inspection
Services®
Commercial
&
Environmental
Stuart
Professional
Park
1136
East
Stuart
Street,
Suite
4204
Fort
Collins,
CO
80525-1193
(970)
482-1976
•
Fax
(970)
482-3388
E-mail:
bill.warren@nationalinspection.net
www.nationalinspection.net
WILLIAM
J.
WARREN
-
ENVIRONMENTAL
PROFESSIONAL
ENVIRONMENTAL
AND
COMMERCIAL
BUILDING
INSPECTION
PROFESSIONAL
STATEMENT
OF
QUALIFICATIONS:
Education:
Phase
II
Subsurface
Investigation
–
430
North
College
Avenue,
Fort
Collins,
Colorado
80524
December
5,
2011
US
Environmental
protection
Agency
Region
8
Radon
Team
member
US
Environmental
Protection
Agency
Radon
Cooperative
Partnership
Program
member
US
Environmental
Protection
Agency
Building
Air
Quality
Alliance
ASTM
Committee
member
E–50
Environmental
Site
Assessment,
Risk
assessment,
Risk
Management
and
Corrective
Action
ASTM
Committee
member
E–50–02
Phase
II
Subsurface
Investigation
–
430
North
College
Avenue,
Fort
Collins,
Colorado
80524
December
5,
2011
National
Inspection
Services®
Commercial
&
Environmental
Stuart
Professional
Park
1136
East
Stuart
Street,
Suite
4204
Fort
Collins,
CO
80525-1193
(970)
482-1976
•
Fax
(970)
482-3388
E-mail:
bill.warren@nationalinspection.net
www.nationalinspection.net
CLEAVE
BERDZAR
-
ENVIRONMENTAL
PROFESSIONAL
STATEMENT
OF
QUALIFICATIONS:
Education:
Bachelor of Arts Degree, Environmental Studies and Planning; Hazardous
Materials
Management and
Water
Quality,
Sonoma
State
Phase
II
Subsurface
Investigation
–
430
North
College
Avenue,
Fort
Collins,
Colorado
80524
December
5,
2011
Mr. Berdzar has developed geographic information system (GIS) projects consisting of aerial
photography, monitoring well and soil boring inventories, groundwater and
chemical
constituent
contouring
and
product
thickness
gridding.
Mr.
Berdzar
has
also
incorporated
the
drafting
(CAD)
of
base
maps, utilities, equipment and chemical concentration layering in support of various environmental
projects.
Professional
Activities:
• Management
of
over
a
thousand
Phase
I
Environmental
Site
Assessment
projects.
• Management
of
project
budgets.
• Project
estimation,
bidding
and
proposals.
• Technical
Page 77 of 80
Page 78 of 80
Phase
II
Subsurface
Investigation
–
430
North
College
Avenue,
Fort
Collins,
Colorado
80524
December
5,
2011
DISCLAIMER
OF
LIABILITY
Page 79 of 80
Phase
II
Subsurface
Investigation
–
430
North
College
Avenue,
Fort
Collins,
Colorado
80524
December
5,
2011
National
Inspection
Services®
Commercial
&
Environmental
Stuart
Professional
Park
1136
East
Stuart
Street,
Suite
4204
Fort
Collins,
CO
80525-1193
(970)
482-1976
•
Fax
(970)
482-3388
E-mail:
bill.warren@nationalinspection.net
ADDENDUM
TO
AND
DISCLAIMER www.nationalinspection.
OF
LIABILITY net
FOR
ENVIRONMENTAL
INSPECTION
AND
REPORTING
PRACTICES
T
he regarding inspection inspector,
or the
the his attached
attached consultants performed
analysis and
report, staff environmental do
beyond not guarantee
a
reasonable evaluation, or
diligence. warrant the physical ANYTHING site
Test report used devices, in were the preparation supplied equipment by of and an this E.test P.report A. results, approved are if in any, analytical general utilized accordance laboratory.
in the generation
with All the procedures current of this
E.N
ational all collectively P.associated A.
protocols
Inspection
and personnel
for
individually,
inspecting,
Services®, and
for
sampling, vendors
William
laboratory
J.
and do
Warren
analysis not
analysis assume
&
Son,
results,
and
LLC,
reporting. responsibility
or
William
for
any
J.
Warren
financial or liability,
and
or
health clients, shall
be
consequences
and
at
the
noncompliance
risk
and
of
responsibility
subsequent
with
recommended
action
of
the
of
recipient lack
measure
of
action
of
of
recipients
abatement,
by
clients
of
if
the
or
prescribed,
agents
attached
of
report. F
or
further
information
about
the
health
safety
implications
of
the
results
indicated,
please
contact
your
local,
state,
and
federal
building
and
health
officials.
Page 80 of 80
CDN #2627A-019
report
review.
• Client
management.
• Limited
Property
Condition
Assessment
management,
review
and
revision.
• Operation
and
Maintenance
Plans
for
asbestos,
lead-based
paint,
mold
and
PCBs.
• Phase
I
Environmental
Site
Assessments.
• Phase
II
Subsurface
Investigations.
• Site
Characterization
Studies.
• Indoor
Air
Quality
Studies.
• Regulatory
Compliance
Assessments.
• Technical
support
and
coordination
to
sub-contractor
division
and
environmental
staff.
• Database administrator and manager for the Environmental Management System (EMS). Data
management system includes groundwater, soil and air matrices including
field
and
analytical
data.
• Management of well hydraulics and treatment system plants data. Development of data
schematics for multiple treatment systems, management of injection/extraction rates, system
efficiency
and
reporting.
• Hydrological and subsurface analysis including groundwater/concentration contouring and
product
plume
tracking
and
migration.
• Drafting (CAD) support in the areas of base maps, wells, utilities, equipment, and subsurface
hydraulics
and
chemical
concentrations.
• Development
and
management for
Geographic Information System (GIS)
projects in the
areas
of
aerial
photography,
base
maps,
groundwater/analyte
contouring,
and
product
thickness
gridding.
• Website maintenance and development for project deliverables, webGIS and database query
interface
utilities.
• Database
analysis in
query
optimization,
data
modeling,
population
and
modification
of
surface,
subsurface,
and
biological
data.
• Global
Positioning
Systems
(GPS)
data
collection.
• Website design for various Naval Environmental Programs including the San Diego Sand
Replenishment
Project,
the
San
Diego
Naval
Station
Natural
Resources
Program
and
storm
water
projects.
Certifications:
Registered
Environmental
Assessor
(California)
#30058
Certified
Building
Inspector
(Colorado)
#15108
Management
Planner
(Colorado)
#15108
Page 76 of 80
University,
1995
Work
Experience:
Mr. Berdzar has ten years experience in the environmental field involving real estate assessment,
environmental management systems, database administration, geographical information systems,
computer
aided
drafting
and remediation
analysis.
Mr.
Berdzar
has conducted
Phase I
Environmental
Site Assessments, Real Estate Transaction Screens, Regulatory Database Reviews, File/Peer Reviews,
Phase II Subsurface Investigations, Site Characterization Studies, Indoor Air Analysis, Regulatory
Compliance
Assessments
and limited
Property
Condition
Assessments.
Mr.
Berdzar
has
performed
soil,
air,
asbestos,
lead-based
paint,
radon
and
drinking
water
sampling.
Mr. Berdzar has successfully managed over a thousand single and multi-site environmental due
diligence projects
throughout
the
United
States
for
a
broad
range
of
property
types
including
office,
retail, multi-family, hospitality, healthcare, industrial, military, mobile home park and raw land
properties.
Mr.
Berdzar
has
managed these
projects for
national,
regional
and
government
lenders
as
well as law firms, insurance companies and independent investors. Clients have including Lehman
Brothers,
UBS,
Bear
Stearns,
Wachovia,
NorthMarq
Capital,
CBRE
Melody,
Holiday
Fenoglio
Fowler,
HUD,
Fannie
Mae
and
Freddie
Mac.
Mr.
Berdzar
has
performed
hydrologic
and
subsurface
assessment.
Analysis
has
included
groundwater
contouring,
petroleum
hydrocarbon
and
chlorinated
solvent
plume
tracking
and
migration.
Mr.
Berdzar
has
performed
extensive
development
of
environmental
management
systems.
Mr.
Berdzar
has
developed
databases
for
petroleum
hydrocarbon
and
chlorinated
solvent
remediation
projects
and
treatment
systems.
Administration
has
included
the
management
and
build-out
of
field
monitoring
and
laboratory
analysis
data
and
the
development
of
data
schematics
for
treatment
and
monitoring
systems.
Page 75 of 80
Property
Condition
Assessment
ASTM
Committee
member
E–50–04
Biological
Fate,
Risk
Management
&
Corrective
Actions
ASTM
committee
member
E–47–09
Biological
Effects
and
Environmental
Fate
Previous board and panel member of numerous building code, national trade and professional
associations,
and
bank
boards
of
directors
American
Arbitration
Association
Commercial
panel
Addressed numerous real estate and legal groups at seminars, conferences, and conventions on
hazardous P
ublications: I
nspector
speaks
materials,
Newsletter
construction
series
inspection
1998
–
Present
and
environmental
over
100
issues
applications
on
environmental
internationally
hazards, liability
and
quality
issues
Vacant
Movie
Theatre
Inspection
Handbook
–
US
Career
institute
2003
Exhaustive variety of articles on environmental compliance issues, environmental due diligence, and
related
industry
topics
Author
–
Time–Life
“Fix–it–Yourself”
series
William J.
Warren is
a
unique
highly
accomplished individual
with
a
multi-disciplinary
background in
engineering, law, environmental science and building construction technology. Mr.
Warren regularly
contributes
his
time
and
energies
to
various
civic,
community,
and
philanthropic
endeavors.
Mr.
Warren
is an accomplished author, expert witness, and building inspection pioneer. Mr. Warren enjoys a
reputation
as
his
industry’s
most
published
and
recognized
leader
Page 74 of 80
Graduate Program -
Colorado
State
University
1973
- 1975 Environmental Biology, Biochemistry,
Organic
Chemistry,
Microbiology,
Physiology
Graduate
Teaching
Assistant
–
Colorado
State
University
Department
of
Animal
Science
Post
Graduate
–
Oxford
University,
Oxford
England
Advanced
Management
Program,
Harvard
Business
School,
1990
Graduate
–
Harvard
University
School
of
Public
Health
–
Indoor
Environmental
Health
Studies
Program
Work
Experience:
National
Inspection
Services®
–
President,
since
1975,
our
firm
has
produced
over
85,000
written
reports
based on physical inspections, including over 1500 Phase 1 environmental Site assessments, over 500
Phase
2
subsurface
environmental
investigations,
over
500
geotechnical
subsurface
investigations,
over
250 remedial site restoration projects and over 350 appearances as an expert witness in courts
throughout
the
United
States
and
internationally.
Property
condition
assessments
comprise
the
balance
of
our
assignment
library.
Professional
Activities:
White
House
Environmental
Policy
Committee
1992
–
2000HUD
Environmental
Policy
Committee
1988
–
1992
EPA
Indoor
Air
Quality
Industry
panel
1988
–
2002
Recipient:
White
House
Lifetime
Achievement
Award
for
Radon
Gas
educational
efforts
presented
by
President
Bill
Clinton
October
19,
1993
US
Green
Building
Council
formative
panel
Environmental
Education
foundation
–
Board
member
1998
–
present
Environmental
Support
Solutions,
Inc.
–
Board
of
Directors,
NASDAQ
listed
company
Energy
auditing
program
steering
committee
–
‘Energy
Score’
–
City
of
Fort
Collins,
Colorado
Page 73 of 80
Page 29 of 43
Page 39 of 80
Page 28 of 43
Page 38 of 80
Page 27 of 43
Page 37 of 80
Warren
Plans nationalinspection.
Services® net
• Analytical
Results
• CDPHE
Notification
Letter
• Statement
of
Qualifications
• Disclaimer
of
Liability
Page 6 of 80
CDN #2627A-019
the available 10
the
do
following:
not
review
and
appear at
SS-‐the
of 10
the
to
is time
located
be
proposed
located of this
on
in and
the
driveway
proposed
areas
building
associated
addition
with
footprint
the
building
area
addition.
or
in
the
proposed
parking
• The range Management arsenic of 3 exceedance
Guidance mg/kg to
for value 19
Evaluating mg/
appears kg
Arsenic as
to published
be
Concentrations
below the by
naturally the
in CDPHE’s
Soil.
occurring Risk
• The could which benzo(
is be
in attributed
close a)pyrene
proximity to exceedance railroad
to
the
railroad operations value
appears
right-‐based of-‐
to way.
be on
slightly the location
elevated of SS-‐
and 8,
• The its
natural
lead
exceedance
occurrence
appears
and
highly
to
be
variable
slightly
nature
elevated
(pockets)
and
can .
be
attributed
to
RECOMMENDATIONS
B
ased Inspection • The subsurface studies on
Services®
findings the conducted information
sampling
from
recommends
this at
activity
the available
limited
Property
the
and
Phase
following: at
the
should the
II findings
subsurface time be of from provided this
investigation
previous assessment, to
environmental the
and CDPHE National
shallow for
• review determination Based in the
five Property
on
sampling under
the
identification
of should
locations, the
No
Further Voluntary be
any
of
Action conducted
trace
future Cleanup
for
asbestos-‐
soil
the pursuant
disturbance
proposed (VCUP) containing to
construction program
activities the
materials established
performed to
activities.
identified obtain Soil
at a
Characterization
and
Management
Plan
(SCMP).
Page 5 of 80
CDN #2627A-019
in
Fort were
Collins, stored
Colorado under
ANALYTICAL T
he
three
soil
RESULTS
samples
collected
from
the
three
soil
boring
locations
were
analyzed
for organic Methods volatile compounds 6010B, organic 7016A, (compounds SVOCs) and using 7470A, (VOCs) EPA and
Method using asbestos EPA 8270C,
content Method RCRA
using 8260B, 8
Metals
Polarized semi-‐using volatile Light EPA
Microscopy sampling using EPA locations
Method (PLM). 8270C, The were ten analyzed RCRA (10) soil 8
Metals for samples semi-‐using volatile collected EPA
Methods organic from the compounds 6010B, ten (10) 7016A, (shallow SVOCs) and
7470A, R
esults
and from
asbestos the soil
content sampling
using did
Polarized not identify
Light
Microscopy any organic
(compound PLM). or metal
constituents Values T
he Sample Sample CDPHE
(SS-‐SS-‐SS-‐CSEV)
Location
Location 10 8 8
considers
above VOLATILE
for
Worker
the Benzo[Parameter Parameter
a
method Arsenic
regulated
AND Lead
Standards a]pyrene
SEMI-
detection asbestos-‐
with ASBESTOS VOLATILE Result Result METALS
limits
the 0.2.850
(
(847 14 mg/mg/containing
exception
ORGANIC
or kg) kg)
above CSEV CSEV
of material
the
COPOUNDS
the
Worker
Worker
CDPHE
following: as
Standard
Standard 0.800 1.39
Soil 6 having
Evaluation
(
(mg/mg/at least kg) kg)
1% samples 1%)
of asbestos
asbestos
containing content.
content
asbestos Results
were
concentrations
identified from the
in soil
soil
of
at sampling
samples
least
1%
collected did .
Trace not
amounts
from identify
soil
(less any
borings
than soil
SB-‐1
and
SB-‐3
and
from
shallow
sampling
locations
SS-‐5,
SS-‐8,
and
SS-‐9.
Page 4 of 80
CDN #2627A-019
soils
three sand
across
feet with
bgs.
the
Below gravel
Property
three and
were intermittent
feet
characterized
bgs,
the cobbles
soils
as
consisted
silty from
sand the
of
clayey S
AMPLING S
ampling the
Soil
sand
Characterization efforts
ACTIVITIES
with
gravel completed
with
and
intermittent
Management during this investigation
evidence
Plan
(SCMP)
of
landfill
were
that
is
debris. conducted
currently
in-‐pursuant place
for to
the field indications cutting Property. screened
material. of During the suspect
Additionally, soil the cuttings asbestos-‐subsurface
no generated
wind containing
or investigation,
dust from materials
conditions the National drilling were
were activities. observed Inspection
encountered No in Services® the obvious
during soil
the sheeting potable drilling sprayer
in
the activities.
event containing
of
the National
discovery magnesium Inspection
of
suspect chloride Services®
asbestos in the
was event
containing
equipped of encountered
materials
with
plastic
and dust
a
conditions. D
uring the subsurface investigation, air monitoring activities were conducted by
Century portable investigation.
Environmental air pumps The three to
Hygiene air collect samples
LLC. continuous
were
Three analyzed
on-‐air site samples
personnel by phase for
were the contrast duration
equipped
microscopy of
with the
(fibers, count, PCM).
The inclusive provided
PCM
of
method they
asbestos, meet
detects size fiberglass,
all and
fiber shape
cellulose
types definitions.
and
and
does
other The
not fiber-‐
differentiate result like is
particles, a total
between fiber
and
does identified fibers/not cc
at
below imply
0.004
the
and asbestos
Colorado
0.006 was
fibers/
Maximum necessarily cc
respectively.
Allowable present.
However,
Asbestos Two of
Level
the the
third
(MAAL) samples
sample
of
0.were
was 01
identified identified Electron
at Microscopy over
0.011 0.01
fibers/fibers/
(TEM)cc,
just cc, .
The the
slightly
result sample
over
of was
the
the further
MAAL
TEM
of analyzed
analysis
0.01.
Since
identified by
the Transmission
result
27.
was 3
structures/Services® Public notification Health reported mm2
letter and
submitted in the Environment the findings sample.
on
November to
(On Mr. CDPHE) November Brian
16,
via
2011. Long
phone 10,
A of
copy the 2011,
call Colorado
of
the
with National
notification
a Department
subsequent Inspection
letter of
and
associated
results
is
included
in
the
enclosures
section
of
this
report.
Page 3 of 80
CDN #2627A-019
of
mg/at trace two kg amount
and sampling
3,800
of
asbestos
mg/locations kg,
and
was identified
Benzo(
identified a)at pyrene 0.in 48 one
mg/
exceeded subsurface kg and
the 1.8
standard
mg/soil sample kg.
Additionally,
of
0.
which 39
mg/
was kg a
subsequently containing exceeding CDPHE material point Basic based counted Standards on and the <determined 1% for asbestos Groundwater not content to be were result. considered identified
No constituents asbestos-‐ in any
groundwater DRILLLING O
n subsurface semi-‐
November volatile
investigation
ACTIVITIES
samples
9, organic
2011,
collected constituents,
National
at
the
Property
at
Inspection
the metals,
Property.
designed
Services® and asbestos-‐
to
identify
undertook containing
potential
a
limited
volatile materials
Phase
and
II in
subsurface soil addition
borings footprint soils.
(SB-‐1, The
SB-‐located subsurface 2,
and to
SB-‐the 3) investigation south
completed and southeast
in included
the
area of the
of the
the advancement existing
proposed Engines
building of three and
Energy drilling referenced activities Conservation
under
Ticket by contacting Lab
#
building. A130100657 the Utility Underground
issued Notification
on
November utilities Center were
2,
2011. of Colorado located
The
Property prior (UNCC) to
was various completed
marked utility by
by Drilling
UNCC organizations
and/Engineers or
verbal contacted Inc.
confirmation of for Fort this Collins,
of project.
“all Colorado
clear”
The
three
was using
received borings a Geoprobe
by
were
the
7822DT SB-‐was 1
completed
was
high-‐
completed capacity
to
a
total
to
direct
a
depth
total
push
depth
of
15.
machine
of 3
feet
15.2
bgs,
using
feet
and
below
two-‐
SB-‐inch
ground 3
was
push
completed
surface
probe
equipment.
(bgs)
to
a ,
SB-‐
total 2
depth was the
soil
not
of
boring
encountered
16.1
locations feet
bgs.
at
Refusal
any
is
included
of
the
was
three
in
experienced
the
boring
enclosures
locations.
at
16.
section 1
A feet
sampling
of
bgs
this
and
report.
map
groundwater
displaying
S
HALLOW O
n subsurface volatile November
organic
SUBSURFACE sampling 9,
constituents, 2011, activity
EXPLORATORY National
metals, at the Inspection Property
and
ACTIVITIES
asbestos-‐Services® designed containing to also identify undertook
materials potential in a
shallow shallow semi-‐
subsurface ten driveway
(10)
shallow areas soils.
sampling associated The shallow
points with subsurface
(the SS-‐1 building
through investigation addition
SS-‐10)
in included and
the
proposed from the remaining completion
parking areas
and of
located completed throughout
by
hand
using the
a Property.
shovel
to The
a
depth ten
of (10)
approximately shallow sampling
one
foot points
below were
the
Page 2 of 80
CDN CDN##2627A-2214A-019 023
Howes
Colorado Phase
Street
80521
– II
Room Subsurface
410 Investigation and Shallow Subsurface
Sampling
Activity
Colorado
State
University
–
Engines
and
Energy
Conservation
Lab
(EECL)
430
North
College
Avenue
D
ear
Mr. Fort
MacMillan,
Collins,
Colorado
80524
N
ational Research shallow
subsurface Inspection Foundation
sampling Services® to perform
activity
was a
retained limited
of
the
Colorado Phase
by
the II
State subsurface Colorado
University investigation State
Engines University
and and
Energy Colorado. conditions Conservation This in the activity area Lab of was
located the designed proposed
at
430 to construction North investigate College of current Avenue the four-‐
in subsurface story
Fort
Collins, building soil
addition Lab addition,
building,
and to the
in
from
proposed southern
remaining
portion
parking
areas
of
and
located the
driveway
existing
throughout
areas Engines
associated
the
and
Property.
Energy
with
A
Conservation
the
copy
building
of
the
proposed B
ACKGROUND
construction
plan
is
included
in
the
enclosures
section
of
this
report.
T
he utilized to the Property construction
for
industrial was formerly of
applications the power occupied
that plant,
including by portions the Fort
power of the Collins
generation Property Power
were
activities. Plant utilized and
Prior was for
landfilling
purposes.
Based
on
a
Phase
II
Environment
Site
Assessment
completed
at
Page 1 of 80
CDN #2627A-019